1H-7-ethoxycarbonyl-6-methyl-3-phenyl-pyrazolo[5,1-c][1,2,4]triazole

Base Information

• Chemical Name: 1H-7-ethoxycarbonyl-6-methyl-3-phenyl-pyrazolo[5,1-c][1,2,4]triazole
• CAS No.: 30569-45-0
• Molecular Formula: C₁₄H₁₄N₄O₂
• Molecular Weight: 270.291
• Mol file: 30569-45-0.mol

Synonyms:1H-7-ethoxycarbonyl-6-methyl-3-phenyl-pyrazolo[5,1-c][1,2,4]triazole

Chemical Property of 1H-7-ethoxycarbonyl-6-methyl-3-phenyl-pyrazolo[5,1-c][1,2,4]triazole

Chemical Property:

Purity/Quality:

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Technology Process of 1H-7-ethoxycarbonyl-6-methyl-3-phenyl-pyrazolo[5,1-c][1,2,4]triazole

There total 1 articles about 1H-7-ethoxycarbonyl-6-methyl-3-phenyl-pyrazolo[5,1-c][1,2,4]triazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

→ 1H-7-ethoxycarbonyl-6-methyl-3-phenyl-pyrazolo[5,1-c][1,2,4]triazole (30569-45-0)

Guidance literature:

aus dem Ester 2a mit Br2 und NaOCOCH3;

Reference yield: 92.0%

1H-7-ethoxycarbonyl-6-methyl-3-phenyl-pyrazolo[5,1-c][1,2,4]triazole (30569-45-0) + dimethyl sulfate (77-78-1) → 1,6-dimethyl-7-ethoxycarbonyl-3-phenyl-pyrazolo[5,1-c][1,2,4]triazole (927408-45-5)

Guidance literature:

With sodium hydroxide; In N,N-dimethyl-formamide; at 20 ℃; for 1h;

DOI:10.1016/j.tet.2006.11.067

Reference yield: 91.0%

1H-7-ethoxycarbonyl-6-methyl-3-phenyl-pyrazolo[5,1-c][1,2,4]triazole (30569-45-0) + benzyl bromide (100-39-0) → 1-benzyl-7-ethoxycarbonyl-6-methyl-3-phenyl-pyrazolo[5,1-c][1,2,4]triazole

Guidance literature:

With potassium carbonate; potassium iodide; In butanone; at 70 ℃; for 4h;

DOI:10.1016/j.tet.2006.11.067

Downstream raw materials:

7-ethoxycarbonyl-1-ethyl-6-methyl-3-phenyl-pyrazolo[5,1-c][1,2,4]triazole

1,6-dimethyl-7-ethoxycarbonyl-3-phenyl-pyrazolo[5,1-c][1,2,4]triazole