Technology Process of C42H46O8
There total 7 articles about C42H46O8 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
2-methylmercaptoethanol; boron trifluoride diethyl etherate;
In
chloroform;
at 45 ℃;
for 0.666667h;
Yield given;
DOI:10.1039/a700422b
- Guidance literature:
-
Multi-step reaction with 6 steps
1: 72 percent / pyridine / 16 h / Heating
2: 76 percent / p-TsOH, ethylene glycol / CHCl3 / 1.5 h / 50 °C
3: 35 percent / PPh3*HBr / CHCl3 / 96 h / Ambient temperature
4: Bu4NF / tetrahydrofuran / 10 h / 60 °C
5: 61 percent / NaH, Bu4NI / dimethylformamide / 1.) 0 deg C, 1 h, 2.) r.t., 36 h
6: 1-sulfanylpropan-1-ol, BF3*Et2O / CHCl3 / 0.67 h / 45 °C
With
pyridine; 2-methylmercaptoethanol; boron trifluoride diethyl etherate; tetrabutyl ammonium fluoride; triphenylphosphine hydrobromide; tetra-(n-butyl)ammonium iodide; sodium hydride; toluene-4-sulfonic acid; ethylene glycol;
In
tetrahydrofuran; chloroform; N,N-dimethyl-formamide;
DOI:10.1039/a700422b
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 61 percent / NaH, Bu4NI / dimethylformamide / 1.) 0 deg C, 1 h, 2.) r.t., 36 h
2: 1-sulfanylpropan-1-ol, BF3*Et2O / CHCl3 / 0.67 h / 45 °C
With
2-methylmercaptoethanol; boron trifluoride diethyl etherate; tetra-(n-butyl)ammonium iodide; sodium hydride;
In
chloroform; N,N-dimethyl-formamide;
DOI:10.1039/a700422b
