(2S,9S)-7-Benzyl-2-(carbobenzoxyamino)-10-chloro-9-hydroxy-7-azadecanoic acid benzyl ester

Base Information

Chemical Name:(2S,9S)-7-Benzyl-2-(carbobenzoxyamino)-10-chloro-9-hydroxy-7-azadecanoic acid benzyl ester
CAS No.:151963-67-6
Molecular Formula:C₃₁H₃₇ClN₂O₅
Molecular Weight:553.098
Hs Code.:

Synonyms:(2S,9S)-7-Benzyl-2-(carbobenzoxyamino)-10-chloro-9-hydroxy-7-azadecanoic acid benzyl ester

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Chemical Property of (2S,9S)-7-Benzyl-2-(carbobenzoxyamino)-10-chloro-9-hydroxy-7-azadecanoic acid benzyl ester

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Technology Process of (2S,9S)-7-Benzyl-2-(carbobenzoxyamino)-10-chloro-9-hydroxy-7-azadecanoic acid benzyl ester

There total 3 articles about (2S,9S)-7-Benzyl-2-(carbobenzoxyamino)-10-chloro-9-hydroxy-7-azadecanoic acid benzyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 67843-74-7,24969-06-0,13403-37-7
(S)-epichlorohydrin

: 78767-79-0
N^ε-benzyl-N^α-carbobenzoxy-L-lysine benzyl ester

: (2S,9S)-7-Benzyl-2-(carbobenzoxyamino)-9,10-epoxy-7-azadecanoic acid benzyl ester

: 151963-67-6
(2S,9S)-7-Benzyl-2-(carbobenzoxyamino)-10-chloro-9-hydroxy-7-azadecanoic acid benzyl ester

Guidance literature:: Ambient temperature;
DOI:10.1021/jo00076a048

Reference yield:

: 100-52-7
benzaldehyde

: 151963-67-6
(2S,9S)-7-Benzyl-2-(carbobenzoxyamino)-10-chloro-9-hydroxy-7-azadecanoic acid benzyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) Na₂CO₃, 2.) NaBH₃CN / 1.) EtOH, 23 deg C, 30 min, 2.) room temp., overnight

2: 75 percent / Ambient temperature

With sodium cyanoborohydride; sodium carbonate;
DOI:10.1021/jo00076a048

Reference yield:

: 5361-91-1
N_α-benzyloxycarbonyl-L-lysine benzyl ester p-toluenesulfonate

: 151963-67-6
(2S,9S)-7-Benzyl-2-(carbobenzoxyamino)-10-chloro-9-hydroxy-7-azadecanoic acid benzyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) Na₂CO₃, 2.) NaBH₃CN / 1.) EtOH, 23 deg C, 30 min, 2.) room temp., overnight

2: 75 percent / Ambient temperature

With sodium cyanoborohydride; sodium carbonate;
DOI:10.1021/jo00076a048