4,4',4''-trihydroxy-3,3',3''-tricarbomethoxy-5,5',5''-trimethyltriphenylmethane

Base Information

Chemical Name:4,4',4''-trihydroxy-3,3',3''-tricarbomethoxy-5,5',5''-trimethyltriphenylmethane
CAS No.:130883-73-7
Molecular Formula:C₂₈H₂₈O₉
Molecular Weight:508.525
Hs Code.:

Synonyms:4,4',4''-trihydroxy-3,3',3''-tricarbomethoxy-5,5',5''-trimethyltriphenylmethane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4,4',4''-trihydroxy-3,3',3''-tricarbomethoxy-5,5',5''-trimethyltriphenylmethane

Chemical Property:

Purity/Quality:

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Technology Process of 4,4',4''-trihydroxy-3,3',3''-tricarbomethoxy-5,5',5''-trimethyltriphenylmethane

There total 4 articles about 4,4',4''-trihydroxy-3,3',3''-tricarbomethoxy-5,5',5''-trimethyltriphenylmethane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 186581-53-3,908094-01-9,334-88-3
diazomethane

: 129749-43-5
5,5',5''-tricarboxy-4,4',4''-trihydroxy-3,3',3''-trimethyltriphenylmethane

: 130883-73-7
4,4',4''-trihydroxy-3,3',3''-tricarbomethoxy-5,5',5''-trimethyltriphenylmethane

Guidance literature:: In diethyl ether; at 5 ℃; for 24h;
DOI:10.1021/jm00105a053

Reference yield:

: 83-40-9
3-methylsalicylic acid

: 130883-73-7
4,4',4''-trihydroxy-3,3',3''-tricarbomethoxy-5,5',5''-trimethyltriphenylmethane

Guidance literature:: Multi-step reaction with 4 steps

1: 99 percent / 25percent H₂SO₄ / 12 h / 90 °C

2: 90 percent / concd. H₂SO₄, NaNO₂ / 16 h / Ambient temperature

3: 95 percent / H₂ / 10percent Pd/C / methanol / 48 h / 4550.9 Torr

4: 94 percent / diethyl ether / 24 h / 5 °C

With sulfuric acid; hydrogen; sodium nitrite; palladium on activated charcoal; In methanol; diethyl ether;
DOI:10.1021/jm00105a053

Reference yield:

: 2581-36-4
3,3'-dicarboxy-4,4'-dihydroxy-5,5'-dimethyldiphenylmethane

: 130883-73-7
4,4',4''-trihydroxy-3,3',3''-tricarbomethoxy-5,5',5''-trimethyltriphenylmethane

Guidance literature:: Multi-step reaction with 3 steps

1: 90 percent / concd. H₂SO₄, NaNO₂ / 16 h / Ambient temperature

2: 95 percent / H₂ / 10percent Pd/C / methanol / 48 h / 4550.9 Torr

3: 94 percent / diethyl ether / 24 h / 5 °C

With sulfuric acid; hydrogen; sodium nitrite; palladium on activated charcoal; In methanol; diethyl ether;
DOI:10.1021/jm00105a053