C₃₇H₄₉N₃O₉S₂Si

Base Information

Chemical Name:C₃₇H₄₉N₃O₉S₂Si
CAS No.:1355952-10-1
Molecular Formula:C₃₇H₄₉N₃O₉S₂Si
Molecular Weight:772.028
Hs Code.:

C<sub>37</sub>H<sub>49</sub>N<sub>3</sub>O<sub>9</sub>S<sub>2</sub>Si

Synonyms:C₃₇H₄₉N₃O₉S₂Si

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Chemical Property of C₃₇H₄₉N₃O₉S₂Si

Chemical Property:

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Technology Process of C₃₇H₄₉N₃O₉S₂Si

There total 10 articles about C₃₇H₄₉N₃O₉S₂Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 202753-56-8
2-(1H-4-bromoindol-3-yl)-ethanol

: 1355952-10-1
C₃₇H₄₉N₃O₉S₂Si

Guidance literature:: Multi-step reaction with 9 steps

1.1: dmap; triethylamine / dichloromethane / 10 h / 0 - 20 °C

2.1: tetrabutylammomium bromide; sodium hydroxide / dichloromethane; water / 0.17 h / 20 °C

2.2: 0.67 h / 20 °C

3.1: tetrabutylammomium bromide; palladium diacetate; potassium carbonate; tris-(o-tolyl)phosphine / N,N-dimethyl-formamide / 2 h / 100 °C / Inert atmosphere

4.1: methanesulfonamide / water; tert-butyl alcohol / 240 h / 20 °C

5.1: thionyl chloride; triethylamine / dichloromethane / 0.5 h / 0 °C

6.1: sodium azide; tetrabutylammomium bromide / N,N-dimethyl-formamide / 19 h / 90 °C

7.1: toluene-4-sulfonic acid / 3 h / 20 °C

8.1: lithium aluminium tetrahydride / tetrahydrofuran / 1 h / 0 - 20 °C

9.1: dmap; triethylamine / dichloromethane / 12 h / 20 °C

With dmap; lithium aluminium tetrahydride; thionyl chloride; sodium azide; methanesulfonamide; tetrabutylammomium bromide; palladium diacetate; potassium carbonate; toluene-4-sulfonic acid; triethylamine; tris-(o-tolyl)phosphine; sodium hydroxide; In tetrahydrofuran; dichloromethane; water; N,N-dimethyl-formamide; tert-butyl alcohol; 3.1: Heck reaction / 4.1: Sharpless dihydroxylation;
DOI:10.1002/anie.201106205

Reference yield:

: 1355951-99-3
C₂₈H₃₉NO₄SSi

: 1355952-10-1
C₃₇H₄₉N₃O₉S₂Si

Guidance literature:: Multi-step reaction with 6 steps

1: methanesulfonamide / water; tert-butyl alcohol / 240 h / 20 °C

2: thionyl chloride; triethylamine / dichloromethane / 0.5 h / 0 °C

3: sodium azide; tetrabutylammomium bromide / N,N-dimethyl-formamide / 19 h / 90 °C

4: toluene-4-sulfonic acid / 3 h / 20 °C

5: lithium aluminium tetrahydride / tetrahydrofuran / 1 h / 0 - 20 °C

6: dmap; triethylamine / dichloromethane / 12 h / 20 °C

With dmap; lithium aluminium tetrahydride; thionyl chloride; sodium azide; methanesulfonamide; tetrabutylammomium bromide; toluene-4-sulfonic acid; triethylamine; In tetrahydrofuran; dichloromethane; water; N,N-dimethyl-formamide; tert-butyl alcohol; 1: Sharpless dihydroxylation;
DOI:10.1002/anie.201106205

Reference yield:

: 1355952-06-5
C₂₈H₄₀N₄O₅SSi

: 1355952-10-1
C₃₇H₄₉N₃O₉S₂Si

Guidance literature:: Multi-step reaction with 3 steps

1: toluene-4-sulfonic acid / 3 h / 20 °C

2: lithium aluminium tetrahydride / tetrahydrofuran / 1 h / 0 - 20 °C

3: dmap; triethylamine / dichloromethane / 12 h / 20 °C

With dmap; lithium aluminium tetrahydride; toluene-4-sulfonic acid; triethylamine; In tetrahydrofuran; dichloromethane;
DOI:10.1002/anie.201106205