1,4,7,13,16,19-hexakis(p-tolylsulfonyl)-1,4,7,13,16,19-hexaazacyclotetracosane

Base Information

Chemical Name:1,4,7,13,16,19-hexakis(p-tolylsulfonyl)-1,4,7,13,16,19-hexaazacyclotetracosane
CAS No.:56187-01-0
Molecular Formula:C₆₀H₇₈N₆O₁₂S₆
Molecular Weight:1267.71
Hs Code.:

Synonyms:1,4,7,13,16,19-hexakis(p-tolylsulfonyl)-1,4,7,13,16,19-hexaazacyclotetracosane

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Chemical Property of 1,4,7,13,16,19-hexakis(p-tolylsulfonyl)-1,4,7,13,16,19-hexaazacyclotetracosane

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Technology Process of 1,4,7,13,16,19-hexakis(p-tolylsulfonyl)-1,4,7,13,16,19-hexaazacyclotetracosane

There total 8 articles about 1,4,7,13,16,19-hexakis(p-tolylsulfonyl)-1,4,7,13,16,19-hexaazacyclotetracosane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 20.0%

: 52601-80-6
N,N’,N”-tris(p-toluenesulfonyl)diethylenetriamine N,N-disodium salt

: 76102-72-2
6,9,12-tris(p-tolylsulfonyl)-6,9,12-triazaheptadecane-1,17-bis(methanesulfonate)

: 56187-01-0
1,4,7,13,16,19-hexakis(p-tolylsulfonyl)-1,4,7,13,16,19-hexaazacyclotetracosane

Guidance literature:: In N,N-dimethyl-formamide; at 90 ℃; for 2h;
DOI:10.1021/ja00545a063

Reference yield:

: 76102-75-5
1-<5-<2-(tetrahydropyranyloxy)>pentyl>methanesulfonate

: 56187-01-0
1,4,7,13,16,19-hexakis(p-tolylsulfonyl)-1,4,7,13,16,19-hexaazacyclotetracosane

Guidance literature:: Multi-step reaction with 4 steps

1: 90 percent / dimethylformamide / 2 h / 95 °C

2: 90 percent / p-toluenesulfonic acid / aq. ethanol / 5 h / Heating

3: N(C₂H₅)3 / CH₂Cl₂ / 0.5 h / -5 °C

4: 20 percent / dimethylformamide / 2 h / 95 °C

With toluene-4-sulfonic acid; triethylamine; In ethanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/jo00342a007

Reference yield:

: 76102-76-6
6,9,12-tris(p-tolylsulfonyl)-6,9,12-triaza-1,17-bis<(tetrahydropyran-2-yl)oxy>heptadecane

: 56187-01-0
1,4,7,13,16,19-hexakis(p-tolylsulfonyl)-1,4,7,13,16,19-hexaazacyclotetracosane

Guidance literature:: Multi-step reaction with 3 steps

1: 90 percent / p-toluenesulfonic acid / aq. ethanol / 5 h / Heating

2: N(C₂H₅)3 / CH₂Cl₂ / 0.5 h / -5 °C

3: 20 percent / dimethylformamide / 2 h / 95 °C

With toluene-4-sulfonic acid; triethylamine; In ethanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/jo00342a007