(3S,4S)-3-benzylamino-4-hydroxy-5-(t-butyldiphenylsilyl)oxypentanoic acid

Base Information

Chemical Name:(3S,4S)-3-benzylamino-4-hydroxy-5-(t-butyldiphenylsilyl)oxypentanoic acid
CAS No.:171896-94-9
Molecular Formula:C₂₈H₃₅NO₄Si
Molecular Weight:477.676
Hs Code.:

Synonyms:(3S,4S)-3-benzylamino-4-hydroxy-5-(t-butyldiphenylsilyl)oxypentanoic acid

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (3S,4S)-3-benzylamino-4-hydroxy-5-(t-butyldiphenylsilyl)oxypentanoic acid

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Technology Process of (3S,4S)-3-benzylamino-4-hydroxy-5-(t-butyldiphenylsilyl)oxypentanoic acid

There total 3 articles about (3S,4S)-3-benzylamino-4-hydroxy-5-(t-butyldiphenylsilyl)oxypentanoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

: 171896-93-8
(4S,5S)-4-benzylamino-5-((t-butyldiphenylsilyl)oxymethyl)dihydro-2-(3H)furanone

: 171896-94-9
(3S,4S)-3-benzylamino-4-hydroxy-5-(t-butyldiphenylsilyl)oxypentanoic acid

Guidance literature:: With sodium hydroxide; In methanol; Ambient temperature;
DOI:10.1016/0957-4166(96)00255-8

Reference yield:

: 78508-96-0
(5S)-5-(hydroxymethyl)-5H-furan-2-one

: 171896-94-9
(3S,4S)-3-benzylamino-4-hydroxy-5-(t-butyldiphenylsilyl)oxypentanoic acid

Guidance literature:: Multi-step reaction with 2 steps

1: 2.) imidazole / 1.) MeOH, 0 deg C, 36 h, 2.) DMF, RT, 2 d

2: 77 percent / 1 M aq. NaOH / methanol / Ambient temperature

With 1H-imidazole; sodium hydroxide; In methanol;
DOI:10.1016/0957-4166(96)00255-8

Reference yield:

: 58479-61-1
tert-butylchlorodiphenylsilane

: 171896-94-9
(3S,4S)-3-benzylamino-4-hydroxy-5-(t-butyldiphenylsilyl)oxypentanoic acid

Guidance literature:: Multi-step reaction with 2 steps

1: 2.) imidazole / 1.) MeOH, 0 deg C, 36 h, 2.) DMF, RT, 2 d

2: 77 percent / 1 M aq. NaOH / methanol / Ambient temperature

With 1H-imidazole; sodium hydroxide; In methanol;
DOI:10.1016/0957-4166(96)00255-8