(3S,4S)-3-benzylamino-4-((t-butyldimethylsilyl)oxy)-5-((t-butyldiphenyl)silyl)oxypentanoic acid

Base Information

Chemical Name:(3S,4S)-3-benzylamino-4-((t-butyldimethylsilyl)oxy)-5-((t-butyldiphenyl)silyl)oxypentanoic acid
CAS No.:171896-96-1
Molecular Formula:C₃₄H₄₉NO₄Si₂
Molecular Weight:591.938
Hs Code.:

Synonyms:(3S,4S)-3-benzylamino-4-((t-butyldimethylsilyl)oxy)-5-((t-butyldiphenyl)silyl)oxypentanoic acid

Suppliers and Price of (3S,4S)-3-benzylamino-4-((t-butyldimethylsilyl)oxy)-5-((t-butyldiphenyl)silyl)oxypentanoic acid

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of (3S,4S)-3-benzylamino-4-((t-butyldimethylsilyl)oxy)-5-((t-butyldiphenyl)silyl)oxypentanoic acid

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of (3S,4S)-3-benzylamino-4-((t-butyldimethylsilyl)oxy)-5-((t-butyldiphenyl)silyl)oxypentanoic acid

There total 5 articles about (3S,4S)-3-benzylamino-4-((t-butyldimethylsilyl)oxy)-5-((t-butyldiphenyl)silyl)oxypentanoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₄₀H₆₃NO₄Si₃

: 171896-96-1
(3S,4S)-3-benzylamino-4-((t-butyldimethylsilyl)oxy)-5-((t-butyldiphenyl)silyl)oxypentanoic acid

Guidance literature:: With hydrogenchloride; In methanol;
DOI:10.1016/0040-4039(95)01417-G

Reference yield:

: 78508-96-0
(5S)-5-(hydroxymethyl)-5H-furan-2-one

: 171896-96-1
(3S,4S)-3-benzylamino-4-((t-butyldimethylsilyl)oxy)-5-((t-butyldiphenyl)silyl)oxypentanoic acid

Guidance literature:: Multi-step reaction with 3 steps

1: 2.) imidazole / 1.) MeOH, 0 deg C, 36 h, 2.) DMF, RT, 2 d

2: 77 percent / 1 M aq. NaOH / methanol / Ambient temperature

3: Et₃N, dimethylaminopyridine / dimethylformamide / 20 h / Ambient temperature

With 1H-imidazole; dmap; sodium hydroxide; triethylamine; In methanol; N,N-dimethyl-formamide;
DOI:10.1016/0957-4166(96)00255-8

Reference yield:

: 58479-61-1
tert-butylchlorodiphenylsilane

: 171896-96-1
(3S,4S)-3-benzylamino-4-((t-butyldimethylsilyl)oxy)-5-((t-butyldiphenyl)silyl)oxypentanoic acid

Guidance literature:: Multi-step reaction with 3 steps

1: 2.) imidazole / 1.) MeOH, 0 deg C, 36 h, 2.) DMF, RT, 2 d

2: 77 percent / 1 M aq. NaOH / methanol / Ambient temperature

3: Et₃N, dimethylaminopyridine / dimethylformamide / 20 h / Ambient temperature

With 1H-imidazole; dmap; sodium hydroxide; triethylamine; In methanol; N,N-dimethyl-formamide;
DOI:10.1016/0957-4166(96)00255-8