benzene-1,2-diethanethiol

Base Information

Chemical Name:benzene-1,2-diethanethiol
CAS No.:112453-80-2
Molecular Formula:C₁₀H₁₄S₂
Molecular Weight:198.353
Hs Code.:

Synonyms:benzene-1,2-diethanethiol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of benzene-1,2-diethanethiol

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Technology Process of benzene-1,2-diethanethiol

There total 3 articles about benzene-1,2-diethanethiol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 17378-99-3
2,2’-(1,2-phenylene)diethanol

: 112453-80-2
benzene-1,2-diethanethiol

Guidance literature:: Multi-step reaction with 2 steps

1: diisopropyl azodicarboxylate, Ph₃P / diethyl ether / 26 h / 25 °C

2: 1.5 g / acetyl chloride, ethanol / 13 h / Heating

With ethanol; di-isopropyl azodicarboxylate; acetyl chloride; triphenylphosphine; In diethyl ether;
DOI:10.1021/ja00173a017

Reference yield:

: 7500-53-0
1,2-Phenylenediacetic acid

: 112453-80-2
benzene-1,2-diethanethiol

Guidance literature:: Multi-step reaction with 3 steps

1: LiAlH₄ / tetrahydrofuran / 12 h / 25 °C

2: diisopropyl azodicarboxylate, Ph₃P / diethyl ether / 26 h / 25 °C

3: 1.5 g / acetyl chloride, ethanol / 13 h / Heating

With lithium aluminium tetrahydride; ethanol; di-isopropyl azodicarboxylate; acetyl chloride; triphenylphosphine; In tetrahydrofuran; diethyl ether;
DOI:10.1021/ja00173a017