Phosphorous acid diethyl ester (1S,2R)-2-formyl-cyclohexylmethyl ester

Base Information

Chemical Name:Phosphorous acid diethyl ester (1S,2R)-2-formyl-cyclohexylmethyl ester
CAS No.:130279-51-5
Molecular Formula:C₁₂H₂₃O₄P
Molecular Weight:262.286
Hs Code.:

Synonyms:Phosphorous acid diethyl ester (1S,2R)-2-formyl-cyclohexylmethyl ester

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Chemical Property of Phosphorous acid diethyl ester (1S,2R)-2-formyl-cyclohexylmethyl ester

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Technology Process of Phosphorous acid diethyl ester (1S,2R)-2-formyl-cyclohexylmethyl ester

There total 2 articles about Phosphorous acid diethyl ester (1S,2R)-2-formyl-cyclohexylmethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 201230-82-2
carbon monoxide

: 130279-50-4
(cyclohex-2-enyl)methyl diethyl phosphite

: 130279-51-5
Phosphorous acid diethyl ester (1S,2R)-2-formyl-cyclohexylmethyl ester

Guidance literature:: With dirhodium tetraacetate; hydrogen; In benzene; at 100 ℃; for 44h; under 25857.4 Torr;
DOI:10.1039/c39900000763

Reference yield:

: 103668-33-3,3309-97-5
3-hydroxymethylcyclohexene

: 130279-51-5
Phosphorous acid diethyl ester (1S,2R)-2-formyl-cyclohexylmethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 74 percent / Et₃N / diethyl ether / a) O dge C, 30 min, b) RT, 12 h

2: H₂, tetrakis(acetato)dirhodium(II) (2) / benzene / 25857.4 Torr

With dirhodium tetraacetate; hydrogen; triethylamine; In diethyl ether; benzene;