4-nitro-[1,1':3',1-terphenyl]-5'-phenol

Base Information

Chemical Name:4-nitro-[1,1':3',1-terphenyl]-5'-phenol
CAS No.:98124-35-7
Molecular Formula:C₁₈H₁₃NO₃
Molecular Weight:291.306
Hs Code.:

Synonyms:4-nitro-[1,1':3',1-terphenyl]-5'-phenol

Suppliers and Price of 4-nitro-[1,1':3',1-terphenyl]-5'-phenol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 3 raw suppliers

Chemical Property of 4-nitro-[1,1':3',1-terphenyl]-5'-phenol

Chemical Property:

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Safty Information:

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Technology Process of 4-nitro-[1,1':3',1-terphenyl]-5'-phenol

There total 1 articles about 4-nitro-[1,1':3',1-terphenyl]-5'-phenol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

: 98124-31-3
C₃₆H₂₆NO₃P

: 98124-35-7
4-nitro-[1,1':3',1-terphenyl]-5'-phenol

: 791-28-6
Triphenylphosphine oxide

Guidance literature:: With sodium hydroxide; In ethanol; water; for 15h; Heating;

Reference yield:

: 98124-35-7
4-nitro-[1,1':3',1-terphenyl]-5'-phenol

: 116941-51-6
4-chloro-5′-phenyl-1,1′:3′,1″-terphenyl

Guidance literature:: Multi-step reaction with 4 steps

1.1: dichloromethane / 6 h / 0 - 20 °C / Inert atmosphere

2.1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate / water; ethanol; toluene / 8 h / Reflux

3.1: 5%-palladium/activated carbon; hydrogen / ethanol / 60 °C / 1500.15 Torr / Autoclave

4.1: sulfuric acid; hydrogenchloride / water / 0.17 h / 80 °C

4.2: 4.5 h / 0 - 65 °C

With hydrogenchloride; tetrakis(triphenylphosphine) palladium⁽⁰⁾; sulfuric acid; 5%-palladium/activated carbon; hydrogen; potassium carbonate; In ethanol; dichloromethane; water; toluene;

Reference yield:

: 98124-35-7
4-nitro-[1,1':3',1-terphenyl]-5'-phenol

: 343239-58-7
5′-phenyl-[1,1′:3′,1″-terphenyl]-4-amine

Guidance literature:: Multi-step reaction with 3 steps

1: dichloromethane / 6 h / 0 - 20 °C / Inert atmosphere

2: tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate / water; ethanol; toluene / 8 h / Reflux

3: 5%-palladium/activated carbon; hydrogen / ethanol / 60 °C / 1500.15 Torr / Autoclave

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; 5%-palladium/activated carbon; hydrogen; potassium carbonate; In ethanol; dichloromethane; water; toluene;