2-(2-(4-(3-(1-(4-isobutylphenyl)ethyl)-5-thioxo-1H-1,2,4-triazol-4(5H)-yl)benzoyl)hydrazinyl)-2-oxoethyl nitrate

Base Information

Chemical Name:2-(2-(4-(3-(1-(4-isobutylphenyl)ethyl)-5-thioxo-1H-1,2,4-triazol-4(5H)-yl)benzoyl)hydrazinyl)-2-oxoethyl nitrate
CAS No.:1309588-20-2
Molecular Formula:C₂₃H₂₆N₆O₅S
Molecular Weight:498.563
Hs Code.:

Synonyms:2-(2-(4-(3-(1-(4-isobutylphenyl)ethyl)-5-thioxo-1H-1,2,4-triazol-4(5H)-yl)benzoyl)hydrazinyl)-2-oxoethyl nitrate

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Chemical Property of 2-(2-(4-(3-(1-(4-isobutylphenyl)ethyl)-5-thioxo-1H-1,2,4-triazol-4(5H)-yl)benzoyl)hydrazinyl)-2-oxoethyl nitrate

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Technology Process of 2-(2-(4-(3-(1-(4-isobutylphenyl)ethyl)-5-thioxo-1H-1,2,4-triazol-4(5H)-yl)benzoyl)hydrazinyl)-2-oxoethyl nitrate

There total 7 articles about 2-(2-(4-(3-(1-(4-isobutylphenyl)ethyl)-5-thioxo-1H-1,2,4-triazol-4(5H)-yl)benzoyl)hydrazinyl)-2-oxoethyl nitrate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 1309588-14-4
N'-(2-chloroacetyl)-4-(3-(1-(4-isobutylphenyl)ethyl)-5-thioxo-1H-1,2,4-triazol-4(5H)-yl)benzohydrazide

: 1309588-20-2
2-(2-(4-(3-(1-(4-isobutylphenyl)ethyl)-5-thioxo-1H-1,2,4-triazol-4(5H)-yl)benzoyl)hydrazinyl)-2-oxoethyl nitrate

Guidance literature:: With silver nitrate; In acetonitrile; at 20 ℃; for 3h;
DOI:10.1007/s00044-010-9389-z

Reference yield:

: 306963-81-5
2-(2-(4-isobutylphenyl)propanoyl)hydrazinecarbothioamide

: 1309588-20-2
2-(2-(4-(3-(1-(4-isobutylphenyl)ethyl)-5-thioxo-1H-1,2,4-triazol-4(5H)-yl)benzoyl)hydrazinyl)-2-oxoethyl nitrate

Guidance literature:: Multi-step reaction with 5 steps

1.1: hydrogenchloride; potassium hydroxide / water / Reflux

2.1: ethanol / 4 h / Reflux

3.1: thionyl chloride / 4 h / Reflux

3.2: 6 h / Reflux

4.1: triethylamine / benzene / 10 h / Reflux

5.1: silver nitrate / acetonitrile / 3 h / 20 °C

With hydrogenchloride; thionyl chloride; silver nitrate; triethylamine; potassium hydroxide; In ethanol; water; acetonitrile; benzene;
DOI:10.1007/s00044-010-9389-z

Reference yield:

: 1309588-08-6
4-(3-(1-(4-isobutylphenyl)ethyl)-5-thioxo-1H-1,2,4-triazol-4(5H)-yl)benzohydrazide

: 1309588-20-2
2-(2-(4-(3-(1-(4-isobutylphenyl)ethyl)-5-thioxo-1H-1,2,4-triazol-4(5H)-yl)benzoyl)hydrazinyl)-2-oxoethyl nitrate

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine / benzene / 10 h / Reflux

2: silver nitrate / acetonitrile / 3 h / 20 °C

With silver nitrate; triethylamine; In acetonitrile; benzene;
DOI:10.1007/s00044-010-9389-z