2,2'-di-O-acetyl-3,3'-di-o-benzyl-4,6,4',6'-di-o-benzylidene-α,α'-D-trehalose

Base Information

Chemical Name:2,2'-di-O-acetyl-3,3'-di-o-benzyl-4,6,4',6'-di-o-benzylidene-α,α'-D-trehalose
CAS No.:127072-98-4
Molecular Formula:C₄₄H₄₆O₁₃
Molecular Weight:782.841
Hs Code.:

Synonyms:2,2'-di-O-acetyl-3,3'-di-o-benzyl-4,6,4',6'-di-o-benzylidene-α,α'-D-trehalose

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Chemical Property of 2,2'-di-O-acetyl-3,3'-di-o-benzyl-4,6,4',6'-di-o-benzylidene-α,α'-D-trehalose

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Technology Process of 2,2'-di-O-acetyl-3,3'-di-o-benzyl-4,6,4',6'-di-o-benzylidene-α,α'-D-trehalose

There total 5 articles about 2,2'-di-O-acetyl-3,3'-di-o-benzyl-4,6,4',6'-di-o-benzylidene-α,α'-D-trehalose which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 108-24-7
acetic anhydride

: 127072-92-8
3,3'-di-o-benzyl-4,6,4',6'-di-o-benzylidene-α,α'-D-trehalose

: 127072-98-4
2,2'-di-O-acetyl-3,3'-di-o-benzyl-4,6,4',6'-di-o-benzylidene-α,α'-D-trehalose

Guidance literature:: With iron (III) chloride hexahydrate; In water; at 20 ℃; for 12h;
DOI:10.1039/c0cc04398b

Reference yield:

: 42390-78-3
2,3,4,6,2',3',4',6'-octa-O-trimethylsilyl-α,α-D-trehalose

: 127072-98-4
2,2'-di-O-acetyl-3,3'-di-o-benzyl-4,6,4',6'-di-o-benzylidene-α,α'-D-trehalose

Guidance literature:: Multi-step reaction with 2 steps

1: triethylsilane; iron (III) chloride hexahydrate / dichloromethane; acetonitrile / 3 h / 0 - 20 °C

2: iron (III) chloride hexahydrate / water / 12 h / 20 °C

With triethylsilane; iron (III) chloride hexahydrate; In dichloromethane; water; acetonitrile;
DOI:10.1039/c0cc04398b

Reference yield:

: 99-20-7
TREHALOSE

: 127072-98-4
2,2'-di-O-acetyl-3,3'-di-o-benzyl-4,6,4',6'-di-o-benzylidene-α,α'-D-trehalose

Guidance literature:: Multi-step reaction with 3 steps

1: pyridine / 20 °C

2: triethylsilane; iron (III) chloride hexahydrate / dichloromethane; acetonitrile / 3 h / 0 - 20 °C

3: iron (III) chloride hexahydrate / water / 12 h / 20 °C

With pyridine; triethylsilane; iron (III) chloride hexahydrate; In dichloromethane; water; acetonitrile;
DOI:10.1039/c0cc04398b