Technology Process of 2-(2'',3'',4''-tri-O-acetyl-β-D-xylopyranosyloxy)-2',4,4'-tribenzyloxybibenzyl
There total 3 articles about 2-(2'',3'',4''-tri-O-acetyl-β-D-xylopyranosyloxy)-2',4,4'-tribenzyloxybibenzyl which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
trimethylsilyl trifluoromethanesulfonate;
In
dichloromethane;
at 0 ℃;
for 0.0833333h;
DOI:10.1016/j.bmcl.2008.08.053
- Guidance literature:
-
Multi-step reaction with 2 steps
1: toluene-4-sulfonic acid / tetrahydrofuran; methanol / 2 h / Reflux
2: trimethylsilyl trifluoromethanesulfonate / dichloromethane / 0.08 h / 0 °C
With
trimethylsilyl trifluoromethanesulfonate; toluene-4-sulfonic acid;
In
tetrahydrofuran; methanol; dichloromethane;
DOI:10.1016/j.ejmech.2011.01.065
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 5% Pd(II)/C(eggshell); hydrogen / tetrahydrofuran / 12 h / 20 °C / 760.05 Torr
2: toluene-4-sulfonic acid / tetrahydrofuran; methanol / 2 h / Reflux
3: trimethylsilyl trifluoromethanesulfonate / dichloromethane / 0.08 h / 0 °C
With
trimethylsilyl trifluoromethanesulfonate; 5% Pd(II)/C(eggshell); hydrogen; toluene-4-sulfonic acid;
In
tetrahydrofuran; methanol; dichloromethane;
DOI:10.1016/j.ejmech.2011.01.065
