2-(2'',3'',4''-tri-O-acetyl-β-D-xylopyranosyloxy)-2',4,4'-tribenzyloxybibenzyl

Base Information

Chemical Name:2-(2'',3'',4''-tri-O-acetyl-β-D-xylopyranosyloxy)-2',4,4'-tribenzyloxybibenzyl
CAS No.:1009814-16-7
Molecular Formula:C₄₆H₄₆O₁₁
Molecular Weight:774.865
Hs Code.:

Synonyms:2-(2'',3'',4''-tri-O-acetyl-β-D-xylopyranosyloxy)-2',4,4'-tribenzyloxybibenzyl

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Chemical Property of 2-(2'',3'',4''-tri-O-acetyl-β-D-xylopyranosyloxy)-2',4,4'-tribenzyloxybibenzyl

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Technology Process of 2-(2'',3'',4''-tri-O-acetyl-β-D-xylopyranosyloxy)-2',4,4'-tribenzyloxybibenzyl

There total 3 articles about 2-(2'',3'',4''-tri-O-acetyl-β-D-xylopyranosyloxy)-2',4,4'-tribenzyloxybibenzyl which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 1009814-13-4
2',4,4'-tribenzyloxy-2-hydroxybibenzyl

: 128376-91-0,869848-87-3
2,3,4-tri-O-acetyl-α-D-xylopyranosyl trichloroacetimidate

: 1009814-16-7
2-(2'',3'',4''-tri-O-acetyl-β-D-xylopyranosyloxy)-2',4,4'-tribenzyloxybibenzyl

Guidance literature:: With trimethylsilyl trifluoromethanesulfonate; In dichloromethane; at 0 ℃; for 0.0833333h;
DOI:10.1016/j.bmcl.2008.08.053

Reference yield:

: 1009816-04-9
2',4,4'-tribenzyloxy-2-(methoxymethoxy)bibenzyl

: 1009814-16-7
2-(2'',3'',4''-tri-O-acetyl-β-D-xylopyranosyloxy)-2',4,4'-tribenzyloxybibenzyl

Guidance literature:: Multi-step reaction with 2 steps

1: toluene-4-sulfonic acid / tetrahydrofuran; methanol / 2 h / Reflux

2: trimethylsilyl trifluoromethanesulfonate / dichloromethane / 0.08 h / 0 °C

With trimethylsilyl trifluoromethanesulfonate; toluene-4-sulfonic acid; In tetrahydrofuran; methanol; dichloromethane;
DOI:10.1016/j.ejmech.2011.01.065

Reference yield:

: 1009814-10-1
2',4,4'-tribenzyloxy-2-(methoxymethoxy)stilbene

: 1009814-16-7
2-(2'',3'',4''-tri-O-acetyl-β-D-xylopyranosyloxy)-2',4,4'-tribenzyloxybibenzyl

Guidance literature:: Multi-step reaction with 3 steps

1: 5% Pd(II)/C(eggshell); hydrogen / tetrahydrofuran / 12 h / 20 °C / 760.05 Torr

2: toluene-4-sulfonic acid / tetrahydrofuran; methanol / 2 h / Reflux

3: trimethylsilyl trifluoromethanesulfonate / dichloromethane / 0.08 h / 0 °C

With trimethylsilyl trifluoromethanesulfonate; 5% Pd(II)/C(eggshell); hydrogen; toluene-4-sulfonic acid; In tetrahydrofuran; methanol; dichloromethane;
DOI:10.1016/j.ejmech.2011.01.065