cyclopent-3-enyl phenyl thioether

Base Information

Chemical Name:cyclopent-3-enyl phenyl thioether
CAS No.:3467-69-4
Molecular Formula:C₁₁H₁₂S
Molecular Weight:176.282
Hs Code.:

Synonyms:cyclopent-3-enyl phenyl thioether

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Chemical Property of cyclopent-3-enyl phenyl thioether

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Technology Process of cyclopent-3-enyl phenyl thioether

There total 3 articles about cyclopent-3-enyl phenyl thioether which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 36367-85-8
toluene-4-sulfonic acid cyclopent-3-enyl ester

: 108-98-5
thiophenol

: 3467-69-4
cyclopent-3-enyl phenyl thioether

Guidance literature:: With caesium carbonate; In N,N-dimethyl-formamide; at 20 ℃; for 2h; Inert atmosphere;
DOI:10.1039/c1dt10503e

Reference yield:

: 58794-15-3
hepta-1,6-dien-4-yl 4-methylbenzenesulfonate

: 3467-69-4
cyclopent-3-enyl phenyl thioether

Guidance literature:: Multi-step reaction with 2 steps

1: Hoveyda-Grubbs catalyst second generation / dichloromethane / 16 h / 20 °C / Inert atmosphere

2: caesium carbonate / N,N-dimethyl-formamide / 2 h / 20 °C / Inert atmosphere

With Hoveyda-Grubbs catalyst second generation; caesium carbonate; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1039/c1dt10503e

Reference yield:

: 2883-45-6
1, 6-heptadien-4-ol

: 3467-69-4
cyclopent-3-enyl phenyl thioether

Guidance literature:: Multi-step reaction with 3 steps

1: dmap; triethylamine / dichloromethane / 16 h / 40 °C / Inert atmosphere

2: Hoveyda-Grubbs catalyst second generation / dichloromethane / 16 h / 20 °C / Inert atmosphere

3: caesium carbonate / N,N-dimethyl-formamide / 2 h / 20 °C / Inert atmosphere

With dmap; Hoveyda-Grubbs catalyst second generation; caesium carbonate; triethylamine; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1039/c1dt10503e