di(4-{[9-phenylcarbazole-3-methylene-1-phenylhydrazino]-2-hydroxypropyl}-thiophenyl)sulphur

Base Information

Chemical Name:di(4-{[9-phenylcarbazole-3-methylene-1-phenylhydrazino]-2-hydroxypropyl}-thiophenyl)sulphur
CAS No.:1357516-26-7
Molecular Formula:C₆₈H₅₆N₆O₂S₃
Molecular Weight:1085.43
Hs Code.:

Synonyms:di(4-{[9-phenylcarbazole-3-methylene-1-phenylhydrazino]-2-hydroxypropyl}-thiophenyl)sulphur

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of di(4-{[9-phenylcarbazole-3-methylene-1-phenylhydrazino]-2-hydroxypropyl}-thiophenyl)sulphur

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Technology Process of di(4-{[9-phenylcarbazole-3-methylene-1-phenylhydrazino]-2-hydroxypropyl}-thiophenyl)sulphur

There total 4 articles about di(4-{[9-phenylcarbazole-3-methylene-1-phenylhydrazino]-2-hydroxypropyl}-thiophenyl)sulphur which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 19362-77-7
4,4'-dimercaptodiphenyl sulfide

: 1357351-42-8
9-phenylcarbazole-3-carbaldehyde N-(2,3-epoxypropyl)-N-phenylhydrazone

: 1357516-26-7
di(4-{[9-phenylcarbazole-3-methylene-1-phenylhydrazino]-2-hydroxypropyl}-thiophenyl)sulphur

Guidance literature:: With triethylamine; In butanone; at 20 ℃;
DOI:10.1080/15421406.2011.538605

Reference yield:

: 1357516-22-3
9-phenylcarbazole-3-carbaldehyde N-phenylhydrazone

: 1357516-26-7
di(4-{[9-phenylcarbazole-3-methylene-1-phenylhydrazino]-2-hydroxypropyl}-thiophenyl)sulphur

Guidance literature:: Multi-step reaction with 2 steps

1: sodium sulfate; potassium hydroxide / 20 h / 20 °C

2: triethylamine / butanone / 20 °C

With sodium sulfate; triethylamine; potassium hydroxide; In butanone;
DOI:10.1080/15421406.2011.538605

Reference yield:

: 1150-62-5
N-phenylcarbazole

: 1357516-26-7
di(4-{[9-phenylcarbazole-3-methylene-1-phenylhydrazino]-2-hydroxypropyl}-thiophenyl)sulphur

Guidance literature:: Multi-step reaction with 4 steps

1: trichlorophosphate / 0 - 85 °C / Inert atmosphere

2: methanol / 20 °C / Cooling

3: sodium sulfate; potassium hydroxide / 20 h / 20 °C

4: triethylamine / butanone / 20 °C

With sodium sulfate; triethylamine; potassium hydroxide; trichlorophosphate; In methanol; butanone; 1: Vilsmeier formylation;
DOI:10.1080/15421406.2011.538605