9-Phenylcarbazole

Base Information

• Chemical Name: 9-Phenylcarbazole
• CAS No.: 1150-62-5
• Molecular Formula: C18H13N
• Molecular Weight: 243.308
• Hs Code.: 29339900
• European Community (EC) Number: 214-564-2
• NSC Number: 10416
• DSSTox Substance ID: DTXSID50150928
• Nikkaji Number: J80.204B
• Wikidata: Q72501455
• ChEMBL ID: CHEMBL1540340
• Mol file: 1150-62-5.mol

Synonyms:9-Phenylcarbazole;1150-62-5;N-Phenylcarbazole;9-Phenyl-9H-carbazole;9H-Carbazole, 9-phenyl-;Carbazole, 9-phenyl-;N-PHENYLCARBAZOLE HYDROCHLORIDE;MLS000737925;NSC10416;EINECS 214-564-2;MFCD00004965;NSC 10416;SMR000446051;Carbazol, 9-phenyl;9-phenyl carbazole;9-Phenylcarbazole, 97%;9-Phenyl-9H-carbazole #;SCHEMBL31962;cid_70851;CHEMBL1540340;BDBM58094;DTXSID50150928;HMS2780O14;NSC-10416;AKOS015840875;NCGC00246916-01;AC-22292;AS-18732;SY020195;1H-INDOLE-3-CARBOXYLICACIDBENZYLAMIDE;CS-0018847;FT-0633406;P1492;9-Phenylcarbazole, >=99%, purified by sublimation;W-200874

Chemical Property of 9-Phenylcarbazole

Chemical Property:

• Vapor Pressure: 4.16E-07mmHg at 25°C
• Melting Point: 95-97 °C(lit.)
• Refractive Index: 1.643
• Boiling Point: 415.3 °C at 760 mmHg
• Flash Point: 205 °C
• PSA: 4.93000
• Density: 1.11 g/cm³
• LogP: 4.78370
• Storage Temp.: Inert atmosphere,Room Temperature
• Water Solubility.: Slightly soluble in water.
• XLogP3: 5
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 0
• Rotatable Bond Count: 1
• Exact Mass: 243.104799419
• Heavy Atom Count: 19
• Complexity: 285

Purity/Quality:

99% ^*data from raw suppliers

9-Phenylcarbazole ^*data from reagent suppliers

Safty Information:

• Pictogram(s): Xi
• Hazard Codes: Xi
• Statements: 37/38-41
• Safety Statements: 26-39

MSDS Files:

SDS file from LookChem

Total 1 MSDS from other Authors

Useful:

• Chemical Classes: Nitrogen Compounds -> Amines, Polyaromatic
• Canonical SMILES: C1=CC=C(C=C1)N2C3=CC=CC=C3C4=CC=CC=C42
• Uses: 9-Phenylcarbazole has been used in the electrochemical synthesis of poly(9-phenylcarbazole) films via direct anodic oxidation in mixed electrolytes of boron trifluoride diethyl etherate and sulfuric acid.

Technology Process of 9-Phenylcarbazole

There total 94 articles about 9-Phenylcarbazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

[1,1'-biphenyl]-2,2'-iodonium trifluoromethanesulfonate (189999-35-7) + aniline (62-53-3) → N-phenylcarbazole (1150-62-5)

Guidance literature:

With copper diacetate; sodium carbonate; In ethylene glycol; isopropyl alcohol; at 90 ℃; for 16h; Inert atmosphere;

DOI:10.1016/j.ejmech.2013.07.029

Reference yield: 100.0%

N,N-diphenylaminobenzene (603-34-9) → N-phenylcarbazole (1150-62-5)

Guidance literature:

With oxygen; In acetonitrile; Solvent; Kinetics; Quantum yield; UV-irradiation;

DOI:10.1039/d1nj03101e

Reference yield: 99.0%

2,2'-dibromobiphenyl (13029-09-9) + aniline (62-53-3) → N-phenylcarbazole (1150-62-5)

Guidance literature:

With (6-Dipp)PdCl₂-SPhos; sodium t-butanolate; In neat (no solvent); at 110 ℃; for 24h; Inert atmosphere;

DOI:10.1039/c9dt00216b

upstream raw materials:

9-phenyl-6,7,8,9-tetrahydro-5H-carbazole

iodobenzene

9H-carbazole

dichloromethane

Downstream raw materials:

2-(9H-carbazol-9-yl)benzoic acid

2-carbazol-9-yl-isophthalic acid

3,6-dibromo-9-(4-bromophenyl)-9H-carbazole

dihydro-1,4 phenyl-9 carbazole

Refernces

Synthesis, characterization and photoconductive properties of optically active methacrylic polymers bearing side-chain 9-phenylcarbazole moieties

10.1016/j.polymer.2009.11.054

This study investigates the synthesis, properties, and photoconductivity of novel optically active methacrylic polymers containing 9-phenylcarbazole side chains. The researchers synthesized two new monomers, (S)-(t)-2-methacryloyloxy-N-[4-(9-carbazolyl)phenyl]succinimide [(S)-(t)-MCPS] and (S)-(t)-3-methacryloyloxy-N-[4-(9-carbazolyl)phenyl]pyrrolidine [(S)-(t)-MCPP], and their corresponding homopolymers. These polymers were characterized using various techniques, including NMR, FT-IR, and UV-Vis spectroscopy. The study found that the chiroptical properties of the chiral polymers were higher than those of the monomers, indicating that the overall optical activity is mainly due to the conformational dissymmetry of the macromolecules. The polymers exhibited high thermal stability and glass transition temperatures, making them suitable for optoelectronic applications. The photoconductivity measurements revealed that the presence of a flexible spacer between the main chain and the carbazole chromophore enhances carrier transport via hopping, improving the photoconductive properties.

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