Technology Process of C16H19N5O2
There total 5 articles about C16H19N5O2 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
5%-palladium/activated carbon; hydrogen;
In
methanol;
at 20 ℃;
under 11251.1 Torr;
Inert atmosphere;
Autoclave;
DOI:10.1039/c4cc00752b
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: potassium carbonate / N,N-dimethyl-formamide / 4 h / Reflux; Inert atmosphere
2.1: triethylamine / dichloromethane / 20 °C / Inert atmosphere
3.1: sodium hydride / mineral oil; tetrahydrofuran / 0.5 h / 40 °C / Inert atmosphere
3.2: 12.5 h / 75 °C / Inert atmosphere
4.1: 5%-palladium/activated carbon; hydrogen / methanol / 20 °C / 11251.1 Torr / Inert atmosphere; Autoclave
With
5%-palladium/activated carbon; hydrogen; sodium hydride; potassium carbonate; triethylamine;
In
tetrahydrofuran; methanol; dichloromethane; N,N-dimethyl-formamide; mineral oil;
DOI:10.1039/c4cc00752b
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: sodium hydride / mineral oil; tetrahydrofuran / 0.5 h / 40 °C / Inert atmosphere
1.2: 12.5 h / 75 °C / Inert atmosphere
2.1: 5%-palladium/activated carbon; hydrogen / methanol / 20 °C / 11251.1 Torr / Inert atmosphere; Autoclave
With
5%-palladium/activated carbon; hydrogen; sodium hydride;
In
tetrahydrofuran; methanol; mineral oil;
DOI:10.1039/c4cc00752b