Phenyl-acetic acid 4-chloro-2-phenylacetylamino-benzyl ester

Base Information

Chemical Name:Phenyl-acetic acid 4-chloro-2-phenylacetylamino-benzyl ester
CAS No.:1026433-37-3
Molecular Formula:C₂₃H₂₀ClNO₃
Molecular Weight:393.87
Hs Code.:

Synonyms:Phenyl-acetic acid 4-chloro-2-phenylacetylamino-benzyl ester

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Chemical Property of Phenyl-acetic acid 4-chloro-2-phenylacetylamino-benzyl ester

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Technology Process of Phenyl-acetic acid 4-chloro-2-phenylacetylamino-benzyl ester

There total 1 articles about Phenyl-acetic acid 4-chloro-2-phenylacetylamino-benzyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 37585-16-3
(2-amino-4-chlorophenyl)methanol

: 103-80-0
phenylacetyl chloride

: 1026433-37-3
Phenyl-acetic acid 4-chloro-2-phenylacetylamino-benzyl ester

Guidance literature:: With triethylamine; In dichloromethane; for 2h; Ambient temperature;
DOI:10.1021/jm9605492

Reference yield:

: 1026433-37-3
Phenyl-acetic acid 4-chloro-2-phenylacetylamino-benzyl ester

: 150097-77-1
N-(Benzylcarbonyl)-5-chloro-2-hydroxymethylaniline

Guidance literature:: With sodium hydroxide; In methanol; at 50 ℃; for 0.75h;
DOI:10.1021/jm9605492

Reference yield:

: 1026433-37-3
Phenyl-acetic acid 4-chloro-2-phenylacetylamino-benzyl ester

: 7-Chloro-4-ethyl-3-phenyl-1H-quinolin-2-one

Guidance literature:: Multi-step reaction with 4 steps

1: aq. NaOH / methanol / 0.75 h / 50 °C

2: pyridinium chloroformate, 4 Angstroem molecular sieves / CH₂Cl₂ / 1.5 h / Ambient temperature

3: 2.) pyridinium chlorochromate / 1.) THF, Et₂O, RT, 16 h, 2.) CH₂Cl₂, RT, 90 min

4: EtOH, NaH / 0.5 h / Ambient temperature

With sodium hydroxide; pyridinium chloroformate; ethanol; 4 A molecular sieve; sodium hydride; pyridinium chlorochromate; In methanol; dichloromethane;
DOI:10.1021/jm9605492