(S)-7,7,7-trifluoroheptyl 2-(tert-butoxycarbonylamino)-3-phenylpropanoate

Base Information

Chemical Name:(S)-7,7,7-trifluoroheptyl 2-(tert-butoxycarbonylamino)-3-phenylpropanoate
CAS No.:1422056-46-9
Molecular Formula:C₂₁H₃₀F₃NO₄
Molecular Weight:417.469
Hs Code.:

Synonyms:(S)-7,7,7-trifluoroheptyl 2-(tert-butoxycarbonylamino)-3-phenylpropanoate

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Chemical Property of (S)-7,7,7-trifluoroheptyl 2-(tert-butoxycarbonylamino)-3-phenylpropanoate

Chemical Property:

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Technology Process of (S)-7,7,7-trifluoroheptyl 2-(tert-butoxycarbonylamino)-3-phenylpropanoate

There total 3 articles about (S)-7,7,7-trifluoroheptyl 2-(tert-butoxycarbonylamino)-3-phenylpropanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

: 887144-94-7
Togni's reagent II

: 1422056-69-6
(S)-hex-5-en-1-yl 2-((tert-butoxycarbonyl)amino)-3-phenylpropanoate

: 1422056-46-9
(S)-7,7,7-trifluoroheptyl 2-(tert-butoxycarbonylamino)-3-phenylpropanoate

Guidance literature:: With 4-methyl-morpholine; at 25 ℃; for 48h; Inert atmosphere;
DOI:10.1021/acs.orglett.6b01301

Reference yield: 44.0%

: 1422056-69-6
(S)-hex-5-en-1-yl 2-((tert-butoxycarbonyl)amino)-3-phenylpropanoate

: 129946-88-9
Umemoto's reagent

: 1422056-46-9
(S)-7,7,7-trifluoroheptyl 2-(tert-butoxycarbonylamino)-3-phenylpropanoate

Guidance literature:: With pyridine; methanol; Ru(2,2'-bipyridine)₃Cl₂·6H₂O; at 25 ℃; for 24h; regioselective reaction; Irradiation; Inert atmosphere;
DOI:10.1021/ja401022x

Reference yield:

: 821-41-0
5-Hexen-1-ol

: 13734-34-4
N-tert-butoxycarbonyl-L-phenylalanine

: 1422056-46-9
(S)-7,7,7-trifluoroheptyl 2-(tert-butoxycarbonylamino)-3-phenylpropanoate

Guidance literature:: Multi-step reaction with 2 steps

1: triphenylphosphine; diethylazodicarboxylate / dichloromethane / 18 h / 20 °C

2: Ru(2,2'-bipyridine)₃Cl₂·6H₂O; methanol; pyridine / 24 h / 25 °C / Irradiation; Inert atmosphere

With pyridine; methanol; Ru(2,2'-bipyridine)₃Cl₂·6H₂O; triphenylphosphine; diethylazodicarboxylate; In dichloromethane;
DOI:10.1021/ja401022x