2-acetoxy-3-bromo-6-methoxy-N-<(1-ethyl-2-pyrrolidinyl)methyl>benzamide hydrochloride

Base Information

Chemical Name:2-acetoxy-3-bromo-6-methoxy-N-<(1-ethyl-2-pyrrolidinyl)methyl>benzamide hydrochloride
CAS No.:84225-89-8
Molecular Formula:C₁₇H₂₃BrN₂O₄*ClH
Molecular Weight:435.746
Hs Code.:

Synonyms:2-acetoxy-3-bromo-6-methoxy-N-<(1-ethyl-2-pyrrolidinyl)methyl>benzamide hydrochloride

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Chemical Property of 2-acetoxy-3-bromo-6-methoxy-N-<(1-ethyl-2-pyrrolidinyl)methyl>benzamide hydrochloride

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Technology Process of 2-acetoxy-3-bromo-6-methoxy-N-<(1-ethyl-2-pyrrolidinyl)methyl>benzamide hydrochloride

There total 4 articles about 2-acetoxy-3-bromo-6-methoxy-N-<(1-ethyl-2-pyrrolidinyl)methyl>benzamide hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 26116-12-1
1-ethyl-2-pyrrolidinemethanamine

: Acetic acid 6-bromo-2-chlorocarbonyl-3-methoxy-phenyl ester; hydrochloride

: 84225-89-8
2-acetoxy-3-bromo-6-methoxy-N-<(1-ethyl-2-pyrrolidinyl)methyl>benzamide hydrochloride

Guidance literature:: In toluene; at 20 ℃; for 16h;
DOI:10.1021/jm00147a025

Reference yield:

: 1466-76-8
2-6-dimethoxybenzoic acid

: 84225-89-8
2-acetoxy-3-bromo-6-methoxy-N-<(1-ethyl-2-pyrrolidinyl)methyl>benzamide hydrochloride

Guidance literature:: Multi-step reaction with 4 steps

1: 76 percent / Br₂ / CHCl₃ / 30 h / Ambient temperature

2: 85 percent / conc. H₂SO₄ / 0.37 h / 60 °C

3: SOCl₂ / 16 h / 20 °C

4: 83 percent / toluene / 16 h / 20 °C

With thionyl chloride; sulfuric acid; bromine; In chloroform; toluene;
DOI:10.1021/jm00147a025

Reference yield:

: 84225-86-5
3-bromo-2-hydroxy-6-methoxysalicylic acid

: 84225-89-8
2-acetoxy-3-bromo-6-methoxy-N-<(1-ethyl-2-pyrrolidinyl)methyl>benzamide hydrochloride

Guidance literature:: Multi-step reaction with 3 steps

1: 85 percent / conc. H₂SO₄ / 0.37 h / 60 °C

2: SOCl₂ / 16 h / 20 °C

3: 83 percent / toluene / 16 h / 20 °C

With thionyl chloride; sulfuric acid; In toluene;
DOI:10.1021/jm00147a025