Hydroxy-[2-oxo-4-(2-oxo-propyl)-azetidin-1-yl]-acetic acid tert-butyl ester

Base Information

Chemical Name:Hydroxy-[2-oxo-4-(2-oxo-propyl)-azetidin-1-yl]-acetic acid tert-butyl ester
CAS No.:68485-91-6
Molecular Formula:C₁₂H₁₉NO₅
Molecular Weight:257.287
Hs Code.:

Synonyms:Hydroxy-[2-oxo-4-(2-oxo-propyl)-azetidin-1-yl]-acetic acid tert-butyl ester

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Chemical Property of Hydroxy-[2-oxo-4-(2-oxo-propyl)-azetidin-1-yl]-acetic acid tert-butyl ester

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Technology Process of Hydroxy-[2-oxo-4-(2-oxo-propyl)-azetidin-1-yl]-acetic acid tert-butyl ester

There total 1 articles about Hydroxy-[2-oxo-4-(2-oxo-propyl)-azetidin-1-yl]-acetic acid tert-butyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 68485-90-5
4-(2-oxo-propyl)-azetidin-2-one

: 7633-32-1
tert-butyl glyoxylate

: 68485-91-6
Hydroxy-[2-oxo-4-(2-oxo-propyl)-azetidin-1-yl]-acetic acid tert-butyl ester

Guidance literature:: In benzene; for 4h; Heating;
DOI:10.1039/P19810003242

Reference yield:

: 68485-91-6
Hydroxy-[2-oxo-4-(2-oxo-propyl)-azetidin-1-yl]-acetic acid tert-butyl ester

: 68485-92-7
t-butyl <4-(2-oxopropyl)-2-oxoazetidin-1-yl>triphenylphosphoranylideneacetate

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) 2,6-lutidine, 2.) thionyl chloride / 1) THF, -20 deg C; 2) 20 min

2: 0.255 g / 2,6-lutidine / dioxane / 16 h / Ambient temperature

With 2,6-dimethylpyridine; thionyl chloride; In 1,4-dioxane;
DOI:10.1039/P19810003242