C₂₆H₃₈O₉S

Base Information

Chemical Name:C₂₆H₃₈O₉S
CAS No.:391278-06-1
Molecular Formula:C₂₆H₃₈O₉S
Molecular Weight:526.648
Hs Code.:

C<sub>26</sub>H<sub>38</sub>O<sub>9</sub>S

Synonyms:C₂₆H₃₈O₉S

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Chemical Property of C₂₆H₃₈O₉S

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Technology Process of C₂₆H₃₈O₉S

There total 20 articles about C₂₆H₃₈O₉S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 124-63-0
methanesulfonyl chloride

: 391278-05-0
C₂₅H₃₆O₇

: 391278-06-1
C₂₆H₃₈O₉S

Guidance literature:: With 2,3,5-trimethyl-pyridine; at 0 ℃;
DOI:10.1016/S0040-4039(01)01802-0

Reference yield:

: 2244-16-8,6485-40-1
(S)-p-mentha-6,8-dien-2-one

: 391278-06-1
C₂₆H₃₈O₉S

Guidance literature:: Multi-step reaction with 20 steps

1.1: 92 percent / EtAlCl₂ / toluene

2.1: 89 percent / H⁽¹⁺⁾

3.1: N-methylmorpholine-N-oxide / OsO₄

4.1: NaIO₄

5.1: 90 percent / m-chloroperbenzoic acid / CH₂Cl₂

6.1: 92 percent / H⁽¹⁺⁾

7.1: 100 percent / K₂CO₃ / methanol

8.1: 90 percent / pyridinium chlorochromate; 4 Angstroem MS / CH₂Cl₂

9.1: Et₃N

9.2: 89 percent / -78 °C

10.1: 73 percent / oxone / acetone

11.1: 79 percent / Al(Oi-Pr)3 / toluene

12.1: 96 percent / Et₃N

13.1: 100 percent / -78 °C

14.1: 90 percent / tetrabutylammonium fluoride / tetrahydrofuran

15.1: 86 percent / NaH / 80 °C

16.1: 85 percent / N-methylmorpholine-N-oxide / OsO₄

17.1: 89 percent / NaIO₄

18.1: 70 percent / H₂ / Pd/C

19.1: 94 percent / NaBH₄ / methanol

20.1: 98 percent / collidine / 0 °C

With 2,3,5-trimethyl-pyridine; Oxone; sodium tetrahydroborate; sodium periodate; 4 Angstroem MS; tetrabutyl ammonium fluoride; hydrogen; hydrogen cation; aluminum isopropoxide; sodium hydride; potassium carbonate; 4-methylmorpholine N-oxide; triethylamine; 3-chloro-benzenecarboperoxoic acid; pyridinium chlorochromate; palladium on activated charcoal; osmium(VIII) oxide; ethylaluminum dichloride; In tetrahydrofuran; methanol; dichloromethane; acetone; toluene; 1.1: Diels-Alder reaction / 5.1: Baeyer-Villiger oxidation / 11.1: Oppenauer ox. and Meerwein-Pondorf-Verley red.;
DOI:10.1016/S0040-4039(01)01802-0

Reference yield:

: 391278-09-4
6.8ac-Dimethyl-3c-isopropenyl-Δ⁶-(4arH)-octalon-(1)

: 391278-06-1
C₂₆H₃₈O₉S

Guidance literature:: Multi-step reaction with 19 steps

1.1: 89 percent / H⁽¹⁺⁾

2.1: N-methylmorpholine-N-oxide / OsO₄

3.1: NaIO₄

4.1: 90 percent / m-chloroperbenzoic acid / CH₂Cl₂

5.1: 92 percent / H⁽¹⁺⁾

6.1: 100 percent / K₂CO₃ / methanol

7.1: 90 percent / pyridinium chlorochromate; 4 Angstroem MS / CH₂Cl₂

8.1: Et₃N

8.2: 89 percent / -78 °C

9.1: 73 percent / oxone / acetone

10.1: 79 percent / Al(Oi-Pr)3 / toluene

11.1: 96 percent / Et₃N

12.1: 100 percent / -78 °C

13.1: 90 percent / tetrabutylammonium fluoride / tetrahydrofuran

14.1: 86 percent / NaH / 80 °C

15.1: 85 percent / N-methylmorpholine-N-oxide / OsO₄

16.1: 89 percent / NaIO₄

17.1: 70 percent / H₂ / Pd/C

18.1: 94 percent / NaBH₄ / methanol

19.1: 98 percent / collidine / 0 °C

With 2,3,5-trimethyl-pyridine; Oxone; sodium tetrahydroborate; sodium periodate; 4 Angstroem MS; tetrabutyl ammonium fluoride; hydrogen; hydrogen cation; aluminum isopropoxide; sodium hydride; potassium carbonate; 4-methylmorpholine N-oxide; triethylamine; 3-chloro-benzenecarboperoxoic acid; pyridinium chlorochromate; palladium on activated charcoal; osmium(VIII) oxide; In tetrahydrofuran; methanol; dichloromethane; acetone; toluene; 4.1: Baeyer-Villiger oxidation / 10.1: Oppenauer ox. and Meerwein-Pondorf-Verley red.;
DOI:10.1016/S0040-4039(01)01802-0