3-benzyloxy-5-benzyloxymethyl-2-[1-(4-methoxy-benzyloxymethyl)-2-triisopropylsilanyloxy-ethyl]-phenylamine

Base Information

Chemical Name:3-benzyloxy-5-benzyloxymethyl-2-[1-(4-methoxy-benzyloxymethyl)-2-triisopropylsilanyloxy-ethyl]-phenylamine
CAS No.:312731-86-5
Molecular Formula:C₄₁H₅₅NO₅Si
Molecular Weight:669.977
Hs Code.:

Synonyms:3-benzyloxy-5-benzyloxymethyl-2-[1-(4-methoxy-benzyloxymethyl)-2-triisopropylsilanyloxy-ethyl]-phenylamine

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Chemical Property of 3-benzyloxy-5-benzyloxymethyl-2-[1-(4-methoxy-benzyloxymethyl)-2-triisopropylsilanyloxy-ethyl]-phenylamine

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Technology Process of 3-benzyloxy-5-benzyloxymethyl-2-[1-(4-methoxy-benzyloxymethyl)-2-triisopropylsilanyloxy-ethyl]-phenylamine

There total 10 articles about 3-benzyloxy-5-benzyloxymethyl-2-[1-(4-methoxy-benzyloxymethyl)-2-triisopropylsilanyloxy-ethyl]-phenylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 312731-85-4
[2-(2-benzyloxy-4-benzyloxymethyl-6-nitro-phenyl)-3-(4-methoxy-benzyloxy)-propoxy]-triisopropyl-silane

: 312731-86-5
3-benzyloxy-5-benzyloxymethyl-2-[1-(4-methoxy-benzyloxymethyl)-2-triisopropylsilanyloxy-ethyl]-phenylamine

Guidance literature:: With hydrogen; nickel; In tetrahydrofuran; methanol; for 8.5h;
DOI:10.1021/ja0013879

Reference yield:

: 6635-20-7
isonitrovanillin

: 312731-86-5
3-benzyloxy-5-benzyloxymethyl-2-[1-(4-methoxy-benzyloxymethyl)-2-triisopropylsilanyloxy-ethyl]-phenylamine

Guidance literature:: Multi-step reaction with 10 steps

1: 96 percent / HBr; AcOH / H₂O / 8 h / Heating

2: 85 percent / NaH / dimethylformamide

3: 95 percent / pyridine / CH₂Cl₂ / 0 - 20 °C

4: 80 percent / dimethylformamide / 1 h

5: 94 percent / NaBH₄ / tetrahydrofuran / 0.08 h / 0 °C

6: 86 percent / NaH / tetrahydrofuran; dimethylformamide / 2 h / 20 °C

7: 38 percent / DIBAL-H / toluene / 0.25 h / 0 °C

8: 64 percent / NaH / dimethylformamide / 20 °C

9: 90 percent / 2,6-lutidine / CH₂Cl₂ / 0.33 h / 0 °C

10: 99 percent / H₂ / Raney-Ni / methanol; tetrahydrofuran / 8.5 h

With pyridine; 2,6-dimethylpyridine; sodium tetrahydroborate; hydrogen bromide; hydrogen; sodium hydride; diisobutylaluminium hydride; acetic acid; nickel; In tetrahydrofuran; methanol; dichloromethane; water; N,N-dimethyl-formamide; toluene;
DOI:10.1021/ja0013879

Reference yield:

: 116313-85-0
3,4-dihydroxy-5-nitrobenzaldehyde

: 312731-86-5
3-benzyloxy-5-benzyloxymethyl-2-[1-(4-methoxy-benzyloxymethyl)-2-triisopropylsilanyloxy-ethyl]-phenylamine

Guidance literature:: Multi-step reaction with 9 steps

1: 85 percent / NaH / dimethylformamide

2: 95 percent / pyridine / CH₂Cl₂ / 0 - 20 °C

3: 80 percent / dimethylformamide / 1 h

4: 94 percent / NaBH₄ / tetrahydrofuran / 0.08 h / 0 °C

5: 86 percent / NaH / tetrahydrofuran; dimethylformamide / 2 h / 20 °C

6: 38 percent / DIBAL-H / toluene / 0.25 h / 0 °C

7: 64 percent / NaH / dimethylformamide / 20 °C

8: 90 percent / 2,6-lutidine / CH₂Cl₂ / 0.33 h / 0 °C

9: 99 percent / H₂ / Raney-Ni / methanol; tetrahydrofuran / 8.5 h

With pyridine; 2,6-dimethylpyridine; sodium tetrahydroborate; hydrogen; sodium hydride; diisobutylaluminium hydride; nickel; In tetrahydrofuran; methanol; dichloromethane; N,N-dimethyl-formamide; toluene;
DOI:10.1021/ja0013879