N-phenyl-2-<(phenylseleno)methyl>-4-<(trimethylsilyl)oxy>-2-dodecenamide

Base Information

Chemical Name:N-phenyl-2-<(phenylseleno)methyl>-4-<(trimethylsilyl)oxy>-2-dodecenamide
CAS No.:103633-65-4
Molecular Formula:C₂₈H₄₁NO₂SeSi
Molecular Weight:530.685
Hs Code.:

Synonyms:N-phenyl-2-<(phenylseleno)methyl>-4-<(trimethylsilyl)oxy>-2-dodecenamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-phenyl-2-<(phenylseleno)methyl>-4-<(trimethylsilyl)oxy>-2-dodecenamide

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Technology Process of N-phenyl-2-<(phenylseleno)methyl>-4-<(trimethylsilyl)oxy>-2-dodecenamide

There total 6 articles about N-phenyl-2-<(phenylseleno)methyl>-4-<(trimethylsilyl)oxy>-2-dodecenamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 1666-13-3
diphenyl diselenide

: 103633-62-1
2-methylene-N-phenyl-3-(phenylsulfonyl)-4-<(trimethylsilyl)oxy>dodecanamide

: 103633-65-4
N-phenyl-2-<(phenylseleno)methyl>-4-<(trimethylsilyl)oxy>-2-dodecenamide

Guidance literature:: With sodium tetrahydroborate; In tetrahydrofuran; ethanol; for 2h; Ambient temperature;
DOI:10.1021/jo00262a020

Reference yield: 96.0%

: 23974-72-3
sodium phenylselenide

: 103633-62-1
2-methylene-N-phenyl-3-(phenylsulfonyl)-4-<(trimethylsilyl)oxy>dodecanamide

: 103633-65-4
N-phenyl-2-<(phenylseleno)methyl>-4-<(trimethylsilyl)oxy>-2-dodecenamide

Guidance literature:: In ethanol; at 0 ℃; for 2h;
DOI:10.1016/S0040-4039(00)94941-4

Reference yield:

: 124-19-6
nonan-1-al

: 103633-65-4
N-phenyl-2-<(phenylseleno)methyl>-4-<(trimethylsilyl)oxy>-2-dodecenamide

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) n-BuLi / 1.) THF, HMPA, -78 deg C, 1 h, 2.) -78 deg C, 2 h

2: 83 percent

3: 96 percent / NaBH₄ / ethanol; tetrahydrofuran / 2 h / Ambient temperature

With sodium tetrahydroborate; n-butyllithium; In tetrahydrofuran; ethanol;
DOI:10.1021/jo00262a020