(E)-1-(2-chloro-4-(4-chlorophenyl)butan-2-yl)-2-(4-chlorophenyl)diazene

Base Information

Chemical Name:(E)-1-(2-chloro-4-(4-chlorophenyl)butan-2-yl)-2-(4-chlorophenyl)diazene
CAS No.:1381772-54-8
Molecular Formula:C₁₆H₁₅Cl₃N₂
Molecular Weight:341.667
Hs Code.:

Synonyms:(E)-1-(2-chloro-4-(4-chlorophenyl)butan-2-yl)-2-(4-chlorophenyl)diazene

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Chemical Property of (E)-1-(2-chloro-4-(4-chlorophenyl)butan-2-yl)-2-(4-chlorophenyl)diazene

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Technology Process of (E)-1-(2-chloro-4-(4-chlorophenyl)butan-2-yl)-2-(4-chlorophenyl)diazene

There total 3 articles about (E)-1-(2-chloro-4-(4-chlorophenyl)butan-2-yl)-2-(4-chlorophenyl)diazene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 1381772-18-4
(E)-1-(4-chlorophenyl)-2-(4-(4-chlorophenyl)butan-2-ylidene)hydrazine

: 1381772-54-8
(E)-1-(2-chloro-4-(4-chlorophenyl)butan-2-yl)-2-(4-chlorophenyl)diazene

Guidance literature:: (E)-1-(4-chlorophenyl)-2-(4-(4-chlorophenyl)butan-2-ylidene)hydrazine; With oxalyl dichloride; dimethyl sulfoxide; In tetrahydrofuran; at -78 - -55 ℃; for 0.166667h; Inert atmosphere;

With triethylamine; In tetrahydrofuran; at 25 ℃; for 0.0833333h; Inert atmosphere;
DOI:10.1021/ja303054c

Reference yield:

: 637-87-6
1-Chloro-4-iodobenzene

: 1381772-54-8
(E)-1-(2-chloro-4-(4-chlorophenyl)butan-2-yl)-2-(4-chlorophenyl)diazene

Guidance literature:: Multi-step reaction with 3 steps

1.1: palladium catalyst / Inert atmosphere

2.1: dichloromethane / 17 h / Molecular sieve; Inert atmosphere; Reflux

3.1: oxalyl dichloride; dimethyl sulfoxide / tetrahydrofuran / 0.17 h / -78 - -55 °C / Inert atmosphere

3.2: 0.08 h / 25 °C / Inert atmosphere

With oxalyl dichloride; dimethyl sulfoxide; In tetrahydrofuran; dichloromethane; 1.1: Heck reaction;
DOI:10.1021/ja303054c

Reference yield:

: 3506-75-0
4-(4-chlorophenyl)butan-2-one

: 1381772-54-8
(E)-1-(2-chloro-4-(4-chlorophenyl)butan-2-yl)-2-(4-chlorophenyl)diazene

Guidance literature:: Multi-step reaction with 2 steps

1.1: dichloromethane / 17 h / Molecular sieve; Inert atmosphere; Reflux

2.1: oxalyl dichloride; dimethyl sulfoxide / tetrahydrofuran / 0.17 h / -78 - -55 °C / Inert atmosphere

2.2: 0.08 h / 25 °C / Inert atmosphere

With oxalyl dichloride; dimethyl sulfoxide; In tetrahydrofuran; dichloromethane;
DOI:10.1021/ja303054c