4,5-dihydro-2-phenylcyclopentapyrrole

Base Information

• Chemical Name: 4,5-dihydro-2-phenylcyclopentapyrrole
• CAS No.: 79379-48-9
• Molecular Formula: C₁₃H₁₃N
• Molecular Weight: 183.253

Synonyms:4,5-dihydro-2-phenylcyclopentapyrrole

Chemical Property of 4,5-dihydro-2-phenylcyclopentapyrrole

Chemical Property:

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Technology Process of 4,5-dihydro-2-phenylcyclopentapyrrole

There total 15 articles about 4,5-dihydro-2-phenylcyclopentapyrrole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

2-phenacylcyclopentanone (54669-76-0) → 4,5-dihydro-2-phenylcyclopentapyrrole (79379-48-9)

Guidance literature:

With ammonium acetate; acetic acid; In tetrahydrofuran; at 170 ℃; for 0.25h; Inert atmosphere; Molecular sieve; Microwave irradiation;

DOI:10.1021/ol201133n

Reference yield: 74.0%

1-(1-hydroxy-3-phenylprop-2-yn-1-yl)cyclobutanol → 4,5-dihydro-2-phenylcyclopentapyrrole (79379-48-9)

Guidance literature:

1-(1-hydroxy-3-phenylprop-2-yn-1-yl)cyclobutanol; With (triphenylphosphine)gold(I) chloride; silver trifluoromethanesulfonate; In n-heptane; at 80 ℃; for 1h; Inert atmosphere;

With ammonium acetate; In n-heptane; at 80 ℃; Reagent/catalyst; Solvent; Temperature; Time; Catalytic behavior; Inert atmosphere;

DOI:10.1039/c5cc03979g

Reference yield: 53.0%

7a-morpholin-4-yl-3-phenyl-4,4a,5,6,7,7a-hexahydro-cyclopenta[e][1,2]oxazine (29441-71-2) → 4,5-dihydro-2-phenylcyclopentapyrrole (79379-48-9)

Guidance literature:

With triiron dodecarbonyl; trifluoroacetic acid; In 1,2-dichloro-ethane; at 80 ℃; for 3h;

DOI:10.1246/cl.1981.869

upstream raw materials:

7a-morpholin-4-yl-3-phenyl-4,4a,5,6,7,7a-hexahydro-cyclopenta[e][1,2]oxazine

1-(N-morpholino)cyclopent-1-ene

2-bromo-1-phenyl-ethanone oxime

4-cyclopentylidene-3-phenylisoxazol-5(4H)-one

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