methyl 3-tert-butyl-5-(2,6,6-trimethylcyclohexen-1-yl)-2,4-pentadienoate

Base Information

Chemical Name:methyl 3-tert-butyl-5-(2,6,6-trimethylcyclohexen-1-yl)-2,4-pentadienoate
CAS No.:106140-58-3
Molecular Formula:C₁₉H₃₀O₂
Molecular Weight:290.446
Hs Code.:

Synonyms:methyl 3-tert-butyl-5-(2,6,6-trimethylcyclohexen-1-yl)-2,4-pentadienoate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of methyl 3-tert-butyl-5-(2,6,6-trimethylcyclohexen-1-yl)-2,4-pentadienoate

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Technology Process of methyl 3-tert-butyl-5-(2,6,6-trimethylcyclohexen-1-yl)-2,4-pentadienoate

There total 2 articles about methyl 3-tert-butyl-5-(2,6,6-trimethylcyclohexen-1-yl)-2,4-pentadienoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 73395-75-2
(E)-2-(but-1-en-3-ynyl)-1,3,3-trimethylcyclohex-1-ene

: 106140-58-3
methyl 3-tert-butyl-5-(2,6,6-trimethylcyclohexen-1-yl)-2,4-pentadienoate

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) n-butyllithium / 1.) diethyl ether, hexane, from -70 deg C to -50 deg C, 2.) diethyl ether, hexane, a) -30 deg C, 2 h, b) RT, 4 h

2: 1.) copper(I) iodide / 1.) THF, pentane, -30 deg C, 2.) THF, pentane, -20 deg C, 2 h

With copper(l) iodide; n-butyllithium;
DOI:10.1021/jo00379a016

Reference yield:

: 594-19-4
tert.-butyl lithium

: 106140-56-1
methyl 5-(2,6,6-trimethylcyclohexen-1-yl)-4-penten-2-ynoate

: 106140-58-3
methyl 3-tert-butyl-5-(2,6,6-trimethylcyclohexen-1-yl)-2,4-pentadienoate

Guidance literature:: With copper(l) iodide; Yield given. Multistep reaction; 1.) THF, pentane, -30 deg C, 2.) THF, pentane, -20 deg C, 2 h;
DOI:10.1021/jo00379a016