N,N'-bis(2-trimethylsilylethanesulfonyl)-ramoplanin A₂ aglycon

Base Information

• Chemical Name: N,N'-bis(2-trimethylsilylethanesulfonyl)-ramoplanin A₂ aglycon
• CAS No.: 436848-93-0
• Molecular Formula: C₁₁₇H₁₅₈ClN₂₁O₃₄S₂Si₂
• Molecular Weight: 2558.42

Synonyms:N,N'-bis(2-trimethylsilylethanesulfonyl)-ramoplanin A₂ aglycon

Chemical Property of N,N'-bis(2-trimethylsilylethanesulfonyl)-ramoplanin A₂ aglycon

Chemical Property:

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Technology Process of N,N'-bis(2-trimethylsilylethanesulfonyl)-ramoplanin A₂ aglycon

There total 2 articles about N,N'-bis(2-trimethylsilylethanesulfonyl)-ramoplanin A₂ aglycon which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 20.0%

ramoplanin A2 aglycon dihydrochloride + 2-trimethylsilanyl-ethanesulfonyl chloride (106018-85-3) → N,N'-bis(2-trimethylsilylethanesulfonyl)-ramoplanin A2 aglycon (436848-93-0)

Guidance literature:

With triethylamine; In N,N-dimethyl-formamide; at -20 ℃; for 2h;

DOI:10.1021/ja020237q

Reference yield:

N1-cyclo-[O-[D-Hpg-D-Orn(SES)-D-α-Thr-L-Hpg-D-Hpg-L-α-Thr-L-Phe-D-Orn(SES)-L-Hpg-D-α-Thr-L-Hpg-Gly-L-Leu-D-Ala-L-Chp]-L-threo-HAsn(Trt)]-(2S)-[(2Z,4E)-7-methyl-2,4-octadienoylamino]-N4-trityl-succinamide → N,N'-bis(2-trimethylsilylethanesulfonyl)-ramoplanin A2 aglycon (436848-93-0)

Guidance literature:

With trifluoroacetic acid; In water; at 25 ℃; for 5h;

DOI:10.1021/ja020237q

Reference yield: 83.0%

N,N'-bis(2-trimethylsilylethanesulfonyl)-ramoplanin A2 aglycon (436848-93-0) → ramoplanin A2 aglycon dihydrochloride

Guidance literature:

With hydrogen fluoride; In methoxybenzene; at 0 ℃; for 1.5h;

DOI:10.1021/ja020237q

upstream raw materials:

2-trimethylsilanyl-ethanesulfonyl chloride

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