2-(3,4-Dichlorobenzyl)-1,2-dihydro-3-methyl-1-oxo-4-isoquinoline Acetic Acid

Base Information

Chemical Name:2-(3,4-Dichlorobenzyl)-1,2-dihydro-3-methyl-1-oxo-4-isoquinoline Acetic Acid
CAS No.:79456-18-1
Molecular Formula:C₁₉H₁₅Cl₂NO₃
Molecular Weight:376.239
Hs Code.:

Synonyms:2-(3,4-Dichlorobenzyl)-1,2-dihydro-3-methyl-1-oxo-4-isoquinoline Acetic Acid

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Chemical Property of 2-(3,4-Dichlorobenzyl)-1,2-dihydro-3-methyl-1-oxo-4-isoquinoline Acetic Acid

Chemical Property:

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Technology Process of 2-(3,4-Dichlorobenzyl)-1,2-dihydro-3-methyl-1-oxo-4-isoquinoline Acetic Acid

There total 5 articles about 2-(3,4-Dichlorobenzyl)-1,2-dihydro-3-methyl-1-oxo-4-isoquinoline Acetic Acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 102-47-6
3,4-Dichlorophenylmethyl chloride

: 79456-17-0
1,2-dihydro-3-methyl-1-oxo-4-isoquinoline acetic acid

: 79456-18-1
2-(3,4-Dichlorobenzyl)-1,2-dihydro-3-methyl-1-oxo-4-isoquinoline Acetic Acid

Guidance literature:: DOI:10.1016/S0040-4039(01)81765-2

Reference yield:

: 4165-96-2
3-phenylglutaric acid

: 79456-18-1
2-(3,4-Dichlorobenzyl)-1,2-dihydro-3-methyl-1-oxo-4-isoquinoline Acetic Acid

Guidance literature:: Multi-step reaction with 4 steps

2: 67 percent / K⁽¹⁺⁾OtBu^(1-), BuONO / methanol / 20 °C

3: 89 percent / PCl₃ / ethyl acetate / 1.5 h / 80 °C

With n-Butyl nitrite; potassium tert-butylate; phosphorus trichloride; In methanol; ethyl acetate;
DOI:10.1016/S0040-4039(01)81765-2

Reference yield:

: 79456-12-5
2-methyl-1-oxo-indan-3-acetic acid

: 79456-18-1
2-(3,4-Dichlorobenzyl)-1,2-dihydro-3-methyl-1-oxo-4-isoquinoline Acetic Acid

Guidance literature:: Multi-step reaction with 3 steps

1: 67 percent / K⁽¹⁺⁾OtBu^(1-), BuONO / methanol / 20 °C

2: 89 percent / PCl₃ / ethyl acetate / 1.5 h / 80 °C

With n-Butyl nitrite; potassium tert-butylate; phosphorus trichloride; In methanol; ethyl acetate;
DOI:10.1016/S0040-4039(01)81765-2