N⁽¹⁾-(3,4-bis(benzyloxy)phenethyl)-N⁽⁴⁾-((8-hydroxyquinolin-5-yl)methyl)succinamide

Base Information

• Chemical Name: N⁽¹⁾-(3,4-bis(benzyloxy)phenethyl)-N⁽⁴⁾-((8-hydroxyquinolin-5-yl)methyl)succinamide
• CAS No.: 1094606-83-3
• Molecular Formula: C₃₆H₃₅N₃O₅
• Molecular Weight: 589.691

Synonyms:N⁽¹⁾-(3,4-bis(benzyloxy)phenethyl)-N⁽⁴⁾-((8-hydroxyquinolin-5-yl)methyl)succinamide

Chemical Property of N⁽¹⁾-(3,4-bis(benzyloxy)phenethyl)-N⁽⁴⁾-((8-hydroxyquinolin-5-yl)methyl)succinamide

Chemical Property:

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Technology Process of N⁽¹⁾-(3,4-bis(benzyloxy)phenethyl)-N⁽⁴⁾-((8-hydroxyquinolin-5-yl)methyl)succinamide

There total 1 articles about N⁽¹⁾-(3,4-bis(benzyloxy)phenethyl)-N⁽⁴⁾-((8-hydroxyquinolin-5-yl)methyl)succinamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

5-(aminomethyl)-8-hydroxyquinoline (81748-72-3) + N-[2-(3,4-bis-benzyloxyphenyl)ethyl]succinimic acid 2,5-dioxo-pyrrolidin-1-yl ester (760190-09-8) → N(1)-(3,4-bis(benzyloxy)phenethyl)-N(4)-((8-hydroxyquinolin-5-yl)methyl)succinamide (1094606-83-3)

Guidance literature:

With N-ethyl-N,N-diisopropylamine; In N,N-dimethyl-formamide;

DOI:10.1016/j.tet.2008.09.081

Reference yield: 86.0%

N(1)-(3,4-bis(benzyloxy)phenethyl)-N(4)-((8-hydroxyquinolin-5-yl)methyl)succinamide (1094606-83-3) → N(1)-(3,4-dihydroxyphenethyl)-N(4)-((8-hydroxyquinolin-5-yl)methyl)succinamide (1094606-81-1)

Guidance literature:

With 10% Pd/C; hydrogen; In dimethyl sulfoxide; at 20 ℃;

DOI:10.1016/j.tet.2008.09.081

upstream raw materials:

5-(aminomethyl)-8-hydroxyquinoline

N-[2-(3,4-bis-benzyloxyphenyl)ethyl]succinimic acid 2,5-dioxo-pyrrolidin-1-yl ester

Downstream raw materials:

N⁽¹⁾-(3,4-dihydroxyphenethyl)-N⁽⁴⁾-((8-hydroxyquinolin-5-yl)methyl)succinamide

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