C₄₁H₄₅N₅O₇

Base Information Edit

Chemical Name:C₄₁H₄₅N₅O₇
CAS No.:431052-69-6
Molecular Formula:C₄₁H₄₅N₅O₇
Molecular Weight:719.838
Hs Code.:
Mol file:431052-69-6.mol

C<sub>41</sub>H<sub>45</sub>N<sub>5</sub>O<sub>7</sub>

Synonyms:C₄₁H₄₅N₅O₇

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Chemical Property of C₄₁H₄₅N₅O₇ Edit

Chemical Property:

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Technology Process of C₄₁H₄₅N₅O₇

There total 13 articles about C₄₁H₄₅N₅O₇ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.0%

: 681427-43-0
C₁₈H₁₉N₃O₂

: 431052-68-5
C₂₃H₂₈N₂O₆

: 431052-69-6
C₄₁H₄₅N₅O₇

Guidance literature:: With dmap; 1-hydroxy-7-aza-benzotriazole; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In N,N-dimethyl-formamide;
DOI:10.1016/j.bmcl.2013.06.028

Reference yield:

: 1121-60-4
pyridine-2-carbaldehyde

: 431052-69-6
C₄₁H₄₅N₅O₇

Guidance literature:: Multi-step reaction with 8 steps

1: N,N',N'-trimethylenediamine; n-butyllithium / tetrahydrofuran; hexane; cyclohexane

2: sodium chlorite; sodium dihydrogen phosphate monohydrate; 2-methyl-but-2-ene / tert-butyl alcohol; acetonitrile; water

3: caesium carbonate / N,N-dimethyl-formamide

4: 3-chloro-benzenecarboperoxoic acid / dichloromethane

5: bis-triphenylphosphine-palladium(II) chloride; copper(II) oxide / N,N-dimethyl-formamide / 110 °C

6: trifluoroacetic anhydride / N,N-dimethyl-formamide

7: sodium hydroxide; water / tetrahydrofuran

8: dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; 1-hydroxy-7-aza-benzotriazole / N,N-dimethyl-formamide

With dmap; bis-triphenylphosphine-palladium(II) chloride; sodium chlorite; n-butyllithium; 1-hydroxy-7-aza-benzotriazole; sodium dihydrogen phosphate monohydrate; 2-methyl-but-2-ene; water; caesium carbonate; N,N',N'-trimethylenediamine; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; 3-chloro-benzenecarboperoxoic acid; trifluoroacetic anhydride; copper(II) oxide; sodium hydroxide; In tetrahydrofuran; hexane; dichloromethane; cyclohexane; water; N,N-dimethyl-formamide; acetonitrile; tert-butyl alcohol;
DOI:10.1016/j.bmcl.2013.06.028

Reference yield:

: 431052-64-1
3-(tributylstannyl)picolinaldehyde

: 431052-69-6
C₄₁H₄₅N₅O₇

Guidance literature:: Multi-step reaction with 7 steps

1: sodium chlorite; sodium dihydrogen phosphate monohydrate; 2-methyl-but-2-ene / tert-butyl alcohol; acetonitrile; water

2: caesium carbonate / N,N-dimethyl-formamide

3: 3-chloro-benzenecarboperoxoic acid / dichloromethane

4: bis-triphenylphosphine-palladium(II) chloride; copper(II) oxide / N,N-dimethyl-formamide / 110 °C

5: trifluoroacetic anhydride / N,N-dimethyl-formamide

6: sodium hydroxide; water / tetrahydrofuran

7: dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; 1-hydroxy-7-aza-benzotriazole / N,N-dimethyl-formamide

With dmap; bis-triphenylphosphine-palladium(II) chloride; sodium chlorite; 1-hydroxy-7-aza-benzotriazole; sodium dihydrogen phosphate monohydrate; 2-methyl-but-2-ene; water; caesium carbonate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; 3-chloro-benzenecarboperoxoic acid; trifluoroacetic anhydride; copper(II) oxide; sodium hydroxide; In tetrahydrofuran; dichloromethane; water; N,N-dimethyl-formamide; acetonitrile; tert-butyl alcohol;
DOI:10.1016/j.bmcl.2013.06.028