1,6-anhydro-2-O-(tert-butyldiphenylsilyl)-3,4-dideoxy-β-D-erythro-hex-3-enopyranose

Base Information

Chemical Name:1,6-anhydro-2-O-(tert-butyldiphenylsilyl)-3,4-dideoxy-β-D-erythro-hex-3-enopyranose
CAS No.:138963-09-4
Molecular Formula:C₂₂H₂₆O₃Si
Molecular Weight:366.532
Hs Code.:

Synonyms:1,6-anhydro-2-O-(tert-butyldiphenylsilyl)-3,4-dideoxy-β-D-erythro-hex-3-enopyranose

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Chemical Property of 1,6-anhydro-2-O-(tert-butyldiphenylsilyl)-3,4-dideoxy-β-D-erythro-hex-3-enopyranose

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Technology Process of 1,6-anhydro-2-O-(tert-butyldiphenylsilyl)-3,4-dideoxy-β-D-erythro-hex-3-enopyranose

There total 3 articles about 1,6-anhydro-2-O-(tert-butyldiphenylsilyl)-3,4-dideoxy-β-D-erythro-hex-3-enopyranose which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 58394-28-8
1,6-anhydro-3,4-dideoxy-β-D-erythro-hex-3-enopyranose

: 58479-61-1
tert-butylchlorodiphenylsilane

: 138963-09-4
1,6-anhydro-2-O-(tert-butyldiphenylsilyl)-3,4-dideoxy-β-D-erythro-hex-3-enopyranose

Guidance literature:: With 1H-imidazole; In N,N-dimethyl-formamide; for 3h; Ambient temperature;
DOI:10.3987/COM-91-5872

Reference yield:

: 50705-28-7
1,6-anhydro-3,4-dideoxy-β-D-threo-hex-3-enopyranose

: 138963-09-4
1,6-anhydro-2-O-(tert-butyldiphenylsilyl)-3,4-dideoxy-β-D-erythro-hex-3-enopyranose

Guidance literature:: Multi-step reaction with 3 steps

1: 91.1 percent / triphenylphosphine, diethyl azodicarboxylate / tetrahydrofuran / 48 h / Ambient temperature

2: 98.6 percent / K₂CO₂ / methanol / 1.5 h / Ambient temperature

3: 100 percent / imidazole / dimethylformamide / 3 h / Ambient temperature

With 1H-imidazole; potassium carbonate; triphenylphosphine; diethylazodicarboxylate; In tetrahydrofuran; methanol; N,N-dimethyl-formamide;
DOI:10.3987/COM-91-5872

Reference yield:

: 67307-86-2
2-O-(benzoyl)-1,6-anhydro-3,4-dideoxy-β-D-erythro-hex-3-enopyranose

: 138963-09-4
1,6-anhydro-2-O-(tert-butyldiphenylsilyl)-3,4-dideoxy-β-D-erythro-hex-3-enopyranose

Guidance literature:: Multi-step reaction with 2 steps

1: 98.6 percent / K₂CO₂ / methanol / 1.5 h / Ambient temperature

2: 100 percent / imidazole / dimethylformamide / 3 h / Ambient temperature

With 1H-imidazole; potassium carbonate; In methanol; N,N-dimethyl-formamide;
DOI:10.3987/COM-91-5872