(-)-(5S)-6-<(tert-Butyl)diphenylsilyloxy>-5-(methanesulfonyloxy)hexanoate d'ethyle

Base Information

Chemical Name:(-)-(5S)-6-<(tert-Butyl)diphenylsilyloxy>-5-(methanesulfonyloxy)hexanoate d'ethyle
CAS No.:136113-70-7
Molecular Formula:C₂₅H₃₆O₆SSi
Molecular Weight:492.709
Hs Code.:

Synonyms:(-)-(5S)-6-<(tert-Butyl)diphenylsilyloxy>-5-(methanesulfonyloxy)hexanoate d'ethyle

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (-)-(5S)-6-<(tert-Butyl)diphenylsilyloxy>-5-(methanesulfonyloxy)hexanoate d'ethyle

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Technology Process of (-)-(5S)-6-<(tert-Butyl)diphenylsilyloxy>-5-(methanesulfonyloxy)hexanoate d'ethyle

There total 3 articles about (-)-(5S)-6-<(tert-Butyl)diphenylsilyloxy>-5-(methanesulfonyloxy)hexanoate d'ethyle which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 136113-69-4
(-)-(5S)-<(tert-Butyl)diphenylsilyloxy>-5-hydroxyhexanoate d'ethyle

: 124-63-0
methanesulfonyl chloride

: 136113-70-7
(-)-(5S)-6-<(tert-Butyl)diphenylsilyloxy>-5-(methanesulfonyloxy)hexanoate d'ethyle

Guidance literature:: With triethylamine; In dichloromethane; 1) -5 deg C, 30 min., 2) r.t., 30 min.;
DOI:10.1002/hlca.19910740412

Reference yield:

: 133634-34-1
(-)-(5S)-5,6-Dihydroxyhexanoate d'ethyle

: 136113-70-7
(-)-(5S)-6-<(tert-Butyl)diphenylsilyloxy>-5-(methanesulfonyloxy)hexanoate d'ethyle

Guidance literature:: Multi-step reaction with 2 steps

1: 87 percent / pyridine, 4-(dimethylamino)pyridine / CH₂Cl₂ / 24 h / Ambient temperature

2: 100 percent / Et₃N / CH₂Cl₂ / 1) -5 deg C, 30 min., 2) r.t., 30 min.

With pyridine; dmap; triethylamine; In dichloromethane;
DOI:10.1002/hlca.19910740412

Reference yield:

: 58479-61-1
tert-butylchlorodiphenylsilane

: 136113-70-7
(-)-(5S)-6-<(tert-Butyl)diphenylsilyloxy>-5-(methanesulfonyloxy)hexanoate d'ethyle

Guidance literature:: Multi-step reaction with 2 steps

1: 87 percent / pyridine, 4-(dimethylamino)pyridine / CH₂Cl₂ / 24 h / Ambient temperature

2: 100 percent / Et₃N / CH₂Cl₂ / 1) -5 deg C, 30 min., 2) r.t., 30 min.

With pyridine; dmap; triethylamine; In dichloromethane;
DOI:10.1002/hlca.19910740412