1-tert-butyl-2-methoxy-5-(trifluoromethyl)-4-aminobenzene

Base Information

Chemical Name:1-tert-butyl-2-methoxy-5-(trifluoromethyl)-4-aminobenzene
CAS No.:873055-78-8
Molecular Formula:C₁₂H₁₆F₃NO
Molecular Weight:247.26
Hs Code.:

Synonyms:1-tert-butyl-2-methoxy-5-(trifluoromethyl)-4-aminobenzene

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-tert-butyl-2-methoxy-5-(trifluoromethyl)-4-aminobenzene

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Technology Process of 1-tert-butyl-2-methoxy-5-(trifluoromethyl)-4-aminobenzene

There total 7 articles about 1-tert-butyl-2-methoxy-5-(trifluoromethyl)-4-aminobenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 873055-77-7
1-tert-butyl-2-methoxy-5-(trifluoromethyl)-4-nitrobenzene

: 873055-78-8
1-tert-butyl-2-methoxy-5-(trifluoromethyl)-4-aminobenzene

Guidance literature:: With ammonium formate; Pd-C; In ethanol;

Reference yield:

: 873055-76-6
1-tert-butyl-2-methoxy-5-bromo-4-nitrobenzene

: 873055-78-8
1-tert-butyl-2-methoxy-5-(trifluoromethyl)-4-aminobenzene

Guidance literature:: Multi-step reaction with 2 steps

1: CuI; KF; potassium bromide / N,N-dimethyl-formamide

2: ammonium formate / Pd-C / ethanol

With CuI; KF; ammonium formate; potassium bromide; Pd-C; In ethanol; N,N-dimethyl-formamide;

Reference yield:

: 88-18-6
2-tert-Butylphenol

: 873055-78-8
1-tert-butyl-2-methoxy-5-(trifluoromethyl)-4-aminobenzene

Guidance literature:: Multi-step reaction with 7 steps

1: N-Bromosuccinimide / acetonitrile / 20 °C

2: triethylamine / dichloromethane / 2 h / 0 °C

3: sulfuric acid; potassium nitrate / 3.5 h / 0 °C

4: potassium hydroxide / methanol / 3 h / 20 °C

5: caesium carbonate / N,N-dimethyl-formamide / 4 h / 20 °C

6: copper(l) iodide; potassium fluoride; potassium bromide / N,N-dimethyl-formamide / 125 °C / Sealed tube

7: palladium 10% on activated carbon; ammonium formate / ethanol / 1 h / Reflux

With potassium fluoride; N-Bromosuccinimide; copper(l) iodide; sulfuric acid; palladium 10% on activated carbon; ammonium formate; caesium carbonate; potassium nitrate; triethylamine; potassium bromide; potassium hydroxide; In methanol; ethanol; dichloromethane; N,N-dimethyl-formamide; acetonitrile;