cis-1,2:3,4-diepoxy-1,4-dimethyl-9,10-diphenyl-1,2,3,4-tetrahydroanthracene

Base Information

• Chemical Name: cis-1,2:3,4-diepoxy-1,4-dimethyl-9,10-diphenyl-1,2,3,4-tetrahydroanthracene
• CAS No.: 141901-81-7
• Molecular Formula: C₂₈H₂₂O₂
• Molecular Weight: 390.481

Synonyms:cis-1,2:3,4-diepoxy-1,4-dimethyl-9,10-diphenyl-1,2,3,4-tetrahydroanthracene

Chemical Property of cis-1,2:3,4-diepoxy-1,4-dimethyl-9,10-diphenyl-1,2,3,4-tetrahydroanthracene

Chemical Property:

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Technology Process of cis-1,2:3,4-diepoxy-1,4-dimethyl-9,10-diphenyl-1,2,3,4-tetrahydroanthracene

There total 1 articles about cis-1,2:3,4-diepoxy-1,4-dimethyl-9,10-diphenyl-1,2,3,4-tetrahydroanthracene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.0%

1,4-dimethyl-9,10-diphenylanthracene 1,4-endoperoxide (20153-17-7) → cis-1,2:3,4-diepoxy-1,4-dimethyl-9,10-diphenyl-1,2,3,4-tetrahydroanthracene (141901-81-7)

Guidance literature:

In diethyl ether; at 18 ℃; for 10h; Irradiation;

Reference yield: 42.0%

cis-1,2:3,4-diepoxy-1,4-dimethyl-9,10-diphenyl-1,2,3,4-tetrahydroanthracene (141901-81-7) → 2,5-dimethyl-6,11-diphenyl-4,5-dihydronaphtho<2,3-b>oxepin-4-one (141858-18-6) + 1,5-dimethyl-6,11-diphenyl-1,2-dihydronaphto<2,3-d>oxepin-2-one (141858-17-5) + 1,4-dimethyl-9,10-diphenyl-1,2,3,4-tetrahydroanthracene-2,3-dione (190075-72-0)

Guidance literature:

In diethyl ether; for 5h; Irradiation;

Reference yield: 40.0%

cis-1,2:3,4-diepoxy-1,4-dimethyl-9,10-diphenyl-1,2,3,4-tetrahydroanthracene (141901-81-7) → 1,4-dimethyl-9,10-diphenyl-1,2,3,4-tetrahydroanthracene-2,3-dione (190075-72-0) + 3,4-epoxy-1,4-dimethyl-9,10-diphenyl-1,2,3,4-tetrahydroanthracen-2-one (141858-08-4) + 1-formyl-1,4-dimethyl-5,10-diphenylnaphtho[2,3-c]-2H-pyran

Guidance literature:

With zinc(II) chloride; In benzene; at 0 ℃;

DOI:10.1016/S0040-4039(97)00294-3

upstream raw materials:

1,4-dimethyl-9,10-diphenylanthracene 1,4-endoperoxide

Downstream raw materials:

2,5-dimethyl-6,11-diphenyl-4,5-dihydronaphtho<2,3-b>oxepin-4-one

1,5-dimethyl-6,11-diphenyl-1,2-dihydronaphto<2,3-d>oxepin-2-one

1,4-dimethyl-9,10-diphenyl-1,2,3,4-tetrahydroanthracene-2,3-dione

3,4-epoxy-1,4-dimethyl-9,10-diphenyl-1,2,3,4-tetrahydroanthracen-2-one

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