2,4-dimethoxy-6-(2-oxo-3-phenylsulfanyl-propyl)-benzoic acid ethyl ester

Base Information

Chemical Name:2,4-dimethoxy-6-(2-oxo-3-phenylsulfanyl-propyl)-benzoic acid ethyl ester
CAS No.:867367-70-2
Molecular Formula:C₂₀H₂₂O₅S
Molecular Weight:374.458
Hs Code.:

Synonyms:2,4-dimethoxy-6-(2-oxo-3-phenylsulfanyl-propyl)-benzoic acid ethyl ester

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Chemical Property of 2,4-dimethoxy-6-(2-oxo-3-phenylsulfanyl-propyl)-benzoic acid ethyl ester

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Technology Process of 2,4-dimethoxy-6-(2-oxo-3-phenylsulfanyl-propyl)-benzoic acid ethyl ester

There total 3 articles about 2,4-dimethoxy-6-(2-oxo-3-phenylsulfanyl-propyl)-benzoic acid ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 57749-86-7
ethyl 2,4-dimethoxy-6-methylbenzoate

: 191731-37-0
N-methoxy-N-methyl-2-(phenylthio)acetamide

: 867367-70-2
2,4-dimethoxy-6-(2-oxo-3-phenylsulfanyl-propyl)-benzoic acid ethyl ester

Guidance literature:: ethyl 2,4-dimethoxy-6-methylbenzoate; With lithium diisopropyl amide; In tetrahydrofuran; at -78 ℃; for 0.0833333h;

N-methoxy-N-methyl-2-(phenylthio)acetamide; In tetrahydrofuran; at -78 ℃; for 0.0833333h;
DOI:10.1002/chem.200500160

Reference yield:

: 2524-37-0
ethyl orselinate

: 867367-70-2
2,4-dimethoxy-6-(2-oxo-3-phenylsulfanyl-propyl)-benzoic acid ethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1.1: 98 percent / K₂CO₃ / acetone / 4 h / Heating

2.1: LDA / tetrahydrofuran / 0.08 h / -78 °C

2.2: 88 percent / tetrahydrofuran / 0.08 h / -78 °C

With potassium carbonate; lithium diisopropyl amide; In tetrahydrofuran; acetone;
DOI:10.1002/chem.200500160

Reference yield:

: 108-98-5
thiophenol

: 867367-70-2
2,4-dimethoxy-6-(2-oxo-3-phenylsulfanyl-propyl)-benzoic acid ethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1.1: 95 percent / K₂CO₃ / dimethylformamide / 4 h / 23 °C

2.1: LDA / tetrahydrofuran / 0.08 h / -78 °C

2.2: 88 percent / tetrahydrofuran / 0.08 h / -78 °C

With potassium carbonate; lithium diisopropyl amide; In tetrahydrofuran; N,N-dimethyl-formamide;
DOI:10.1002/chem.200500160