2-benzyloxymethoxymethyl-3-(4-dimethyl-t-butylsilyloxybutyl)cyclohex-2-enon

Base Information

Chemical Name:2-benzyloxymethoxymethyl-3-(4-dimethyl-t-butylsilyloxybutyl)cyclohex-2-enon
CAS No.:119204-06-7
Molecular Formula:C₂₅H₄₀O₄Si
Molecular Weight:432.676
Hs Code.:

Synonyms:2-benzyloxymethoxymethyl-3-(4-dimethyl-t-butylsilyloxybutyl)cyclohex-2-enon

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Chemical Property of 2-benzyloxymethoxymethyl-3-(4-dimethyl-t-butylsilyloxybutyl)cyclohex-2-enon

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Technology Process of 2-benzyloxymethoxymethyl-3-(4-dimethyl-t-butylsilyloxybutyl)cyclohex-2-enon

There total 5 articles about 2-benzyloxymethoxymethyl-3-(4-dimethyl-t-butylsilyloxybutyl)cyclohex-2-enon which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 3587-60-8
Benzyloxymethyl chloride

: 119204-06-7
2-benzyloxymethoxymethyl-3-(4-dimethyl-t-butylsilyloxybutyl)cyclohex-2-enon

Guidance literature:: Multi-step reaction with 3 steps

1: 91 percent / ethyl(di-isopropyl)amine / CH₂Cl₂ / 4 h / Ambient temperature

2: 91 percent / toluene-p-sulphonic acid / 1 h / Ambient temperature

3: 1.) Mg powder / 1.) THF, reflux, 15 h; 2.) THF, -78 deg C, 3 h, then Rt

With toluene-4-sulfonic acid; magnesium; N-ethyl-N,N-diisopropylamine; In dichloromethane;

Reference yield:

: 58310-18-2
1,4-dihydro-2,6-dimethoxybenzoic acid

: 119204-06-7
2-benzyloxymethoxymethyl-3-(4-dimethyl-t-butylsilyloxybutyl)cyclohex-2-enon

Guidance literature:: Multi-step reaction with 4 steps

1: 89 percent / LiAlH₄ / tetrahydrofuran / 0.5 h / Ambient temperature

2: 91 percent / ethyl(di-isopropyl)amine / CH₂Cl₂ / 4 h / Ambient temperature

3: 91 percent / toluene-p-sulphonic acid / 1 h / Ambient temperature

4: 1.) Mg powder / 1.) THF, reflux, 15 h; 2.) THF, -78 deg C, 3 h, then Rt

With lithium aluminium tetrahydride; toluene-4-sulfonic acid; magnesium; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; dichloromethane;

Reference yield:

: 119204-04-5
(2,6-Dimethoxy-cyclohexa-2,5-dienyl)-methanol

: 119204-06-7
2-benzyloxymethoxymethyl-3-(4-dimethyl-t-butylsilyloxybutyl)cyclohex-2-enon

Guidance literature:: Multi-step reaction with 3 steps

1: 91 percent / ethyl(di-isopropyl)amine / CH₂Cl₂ / 4 h / Ambient temperature

2: 91 percent / toluene-p-sulphonic acid / 1 h / Ambient temperature

3: 1.) Mg powder / 1.) THF, reflux, 15 h; 2.) THF, -78 deg C, 3 h, then Rt

With toluene-4-sulfonic acid; magnesium; N-ethyl-N,N-diisopropylamine; In dichloromethane;