(thiophene-2-caboxaldehyde benzhydrazone

Base Information

Chemical Name:(thiophene-2-caboxaldehyde benzhydrazone
CAS No.:113907-55-4
Molecular Formula:C₁₂H₁₀N₂OS
Molecular Weight:230.29
Hs Code.:

Synonyms:(thiophene-2-caboxaldehyde benzhydrazone

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Chemical Property of (thiophene-2-caboxaldehyde benzhydrazone

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Technology Process of (thiophene-2-caboxaldehyde benzhydrazone

There total 1 articles about (thiophene-2-caboxaldehyde benzhydrazone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 498-62-4
3-thiophene carboxaldehyde

: 613-94-5
benzoic acid hydrazide

: 113907-55-4
(thiophene-2-caboxaldehyde benzhydrazone

Guidance literature:: In ethanol; Reflux;
DOI:10.1021/acs.joc.5b02154

Reference yield: 86.0%

: 113907-55-4
(thiophene-2-caboxaldehyde benzhydrazone

: 1118-46-3
Trichlorbutylstannan

: [tin(IV)(chloride)2(butyl)(thiophene-2-caboxaldehyde benzhydrazone(-H))2]

Guidance literature:: With KOH; In methanol; byproducts: KCl; KOH (2 mmol) soln. added dropwise to HTCB (2 mmol) soln. in Schlenk flask, refluxed under N2 for 1 h, SnCl3Bu soln. (2 mmol) added, refluxed for3 h under N2; KCl filtered off, filtrate evapd. at room temp.; elem. anal.;
DOI:10.1016/j.ica.2009.08.010