(Z,Z)-octadeca-9,12-dienoic acid 3-adamantan-1-yl-4'-((E)-2-tert-butoxycarbonylvinyl)biphenyl-4-yl ester

Base Information

Chemical Name:(Z,Z)-octadeca-9,12-dienoic acid 3-adamantan-1-yl-4'-((E)-2-tert-butoxycarbonylvinyl)biphenyl-4-yl ester
CAS No.:1370009-39-4
Molecular Formula:C₄₇H₆₄O₄
Molecular Weight:693.023
Hs Code.:

Synonyms:(Z,Z)-octadeca-9,12-dienoic acid 3-adamantan-1-yl-4'-((E)-2-tert-butoxycarbonylvinyl)biphenyl-4-yl ester

Suppliers and Price of (Z,Z)-octadeca-9,12-dienoic acid 3-adamantan-1-yl-4'-((E)-2-tert-butoxycarbonylvinyl)biphenyl-4-yl ester

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of (Z,Z)-octadeca-9,12-dienoic acid 3-adamantan-1-yl-4'-((E)-2-tert-butoxycarbonylvinyl)biphenyl-4-yl ester

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of (Z,Z)-octadeca-9,12-dienoic acid 3-adamantan-1-yl-4'-((E)-2-tert-butoxycarbonylvinyl)biphenyl-4-yl ester

There total 3 articles about (Z,Z)-octadeca-9,12-dienoic acid 3-adamantan-1-yl-4'-((E)-2-tert-butoxycarbonylvinyl)biphenyl-4-yl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 7459-33-8
linoleyl chloride

: 1232884-73-9
(E)-3-(3'-adamantan-1-yl-4'-hydroxybiphenyl-4-yl)acrylic acid tert-butyl ester

: 1370009-39-4
(Z,Z)-octadeca-9,12-dienoic acid 3-adamantan-1-yl-4'-((E)-2-tert-butoxycarbonylvinyl)biphenyl-4-yl ester

Guidance literature:: With pyridine; at 20 - 50 ℃;

Reference yield:

: 1663-39-4,25232-27-3
tert-Butyl acrylate

: 1370009-39-4
(Z,Z)-octadeca-9,12-dienoic acid 3-adamantan-1-yl-4'-((E)-2-tert-butoxycarbonylvinyl)biphenyl-4-yl ester

Guidance literature:: Multi-step reaction with 2 steps

1: palladium diacetate; triethylamine; tris-(o-tolyl)phosphine / 1 h / 110 °C / Neat (no solvent)

2: pyridine; dmap / 20 °C

With pyridine; dmap; palladium diacetate; triethylamine; tris-(o-tolyl)phosphine; 1: Heck reaction;
DOI:10.1016/j.bmc.2012.01.042

Reference yield:

: 496868-80-5
4-(4'-bromophenyl)-2-(adamantan-1-yl)phenol

: 1370009-39-4
(Z,Z)-octadeca-9,12-dienoic acid 3-adamantan-1-yl-4'-((E)-2-tert-butoxycarbonylvinyl)biphenyl-4-yl ester

Guidance literature:: Multi-step reaction with 2 steps

1: palladium diacetate; triethylamine; tris-(o-tolyl)phosphine / 1 h / 110 °C / Neat (no solvent)

2: pyridine; dmap / 20 °C

With pyridine; dmap; palladium diacetate; triethylamine; tris-(o-tolyl)phosphine; 1: Heck reaction;
DOI:10.1016/j.bmc.2012.01.042