C₄₁H₄₇N₄O₉P

Base Information

Chemical Name:C₄₁H₄₇N₄O₉P
CAS No.:1093849-05-8
Molecular Formula:C₄₁H₄₇N₄O₉P
Molecular Weight:770.819
Hs Code.:

C<sub>41</sub>H<sub>47</sub>N<sub>4</sub>O<sub>9</sub>P

Synonyms:C₄₁H₄₇N₄O₉P

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Chemical Property of C₄₁H₄₇N₄O₉P

Chemical Property:

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Technology Process of C₄₁H₄₇N₄O₉P

There total 12 articles about C₄₁H₄₇N₄O₉P which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1093849-04-7
C₃₂H₃₀N₂O₈

: 102691-36-1
N,N,N',N'-tetraisopropyl 2-cyanoethylphosphorodiamidite

: 1093849-05-8
C₄₁H₄₇N₄O₉P

Guidance literature:: With 1-methyl-1H-imidazole; 1H-tetrazole; In N,N-dimethyl-formamide;

Reference yield:

: 1093848-92-0
C₂₈H₃₂O₇

: 1093849-05-8
C₄₁H₄₇N₄O₉P

Guidance literature:: Multi-step reaction with 11 steps

1.1: dmap; triethylamine / dichloromethane / 0 - 20 °C

2.1: sulfuric acid / water / 2 h / 20 °C

3.1: N,O-bis-(trimethylsilyl)-acetamide / acetonitrile / 0.25 h / 40 °C

3.2: 2 h / Reflux

4.1: potassium carbonate / methanol / 16 h / 20 °C

5.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 16 h / 100 °C

6.1: boron trichloride / dichloromethane / -78 - 0 °C

7.1: 1H-imidazole / N,N-dimethyl-formamide

8.1: 2,3-dicyano-5,6-dichloro-p-benzoquinone; water / dichloromethane

9.1: triethylamine; triethylamine tris(hydrogen fluoride) / tetrahydrofuran

10.1: pyridine

11.1: 1H-tetrazole; 1-methyl-1H-imidazole / N,N-dimethyl-formamide

With pyridine; 1H-imidazole; 1-methyl-1H-imidazole; 1H-tetrazole; dmap; N,O-bis-(trimethylsilyl)-acetamide; sulfuric acid; tetrabutyl ammonium fluoride; water; boron trichloride; potassium carbonate; triethylamine tris(hydrogen fluoride); triethylamine; 2,3-dicyano-5,6-dichloro-p-benzoquinone; In tetrahydrofuran; methanol; dichloromethane; water; N,N-dimethyl-formamide; acetonitrile;

Reference yield:

: 1093848-93-1
C₃₄H₄₆O₇Si

: 1093849-05-8
C₄₁H₄₇N₄O₉P

Guidance literature:: Multi-step reaction with 12 steps

1.1: triethylamine; triethylamine tris(hydrogen fluoride) / tetrahydrofuran / 16 h / 20 °C

2.1: dmap; triethylamine / dichloromethane / 0 - 20 °C

3.1: sulfuric acid / water / 2 h / 20 °C

4.1: N,O-bis-(trimethylsilyl)-acetamide / acetonitrile / 0.25 h / 40 °C

4.2: 2 h / Reflux

5.1: potassium carbonate / methanol / 16 h / 20 °C

6.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 16 h / 100 °C

7.1: boron trichloride / dichloromethane / -78 - 0 °C

8.1: 1H-imidazole / N,N-dimethyl-formamide

9.1: 2,3-dicyano-5,6-dichloro-p-benzoquinone; water / dichloromethane

10.1: triethylamine; triethylamine tris(hydrogen fluoride) / tetrahydrofuran

11.1: pyridine

12.1: 1H-tetrazole; 1-methyl-1H-imidazole / N,N-dimethyl-formamide

With pyridine; 1H-imidazole; 1-methyl-1H-imidazole; 1H-tetrazole; dmap; N,O-bis-(trimethylsilyl)-acetamide; sulfuric acid; tetrabutyl ammonium fluoride; water; boron trichloride; potassium carbonate; triethylamine tris(hydrogen fluoride); triethylamine; 2,3-dicyano-5,6-dichloro-p-benzoquinone; In tetrahydrofuran; methanol; dichloromethane; water; N,N-dimethyl-formamide; acetonitrile;