N-(1-[(4-methylphenyl)sulfonyl]tetrahydro-1H-pyrrol-2-yl)-2-methyl-2-propanesulfinamide

Base Information

Chemical Name:N-(1-[(4-methylphenyl)sulfonyl]tetrahydro-1H-pyrrol-2-yl)-2-methyl-2-propanesulfinamide
CAS No.:918954-35-5
Molecular Formula:C₁₅H₂₄N₂O₃S₂
Molecular Weight:344.499
Hs Code.:

Synonyms:N-(1-[(4-methylphenyl)sulfonyl]tetrahydro-1H-pyrrol-2-yl)-2-methyl-2-propanesulfinamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-(1-[(4-methylphenyl)sulfonyl]tetrahydro-1H-pyrrol-2-yl)-2-methyl-2-propanesulfinamide

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Technology Process of N-(1-[(4-methylphenyl)sulfonyl]tetrahydro-1H-pyrrol-2-yl)-2-methyl-2-propanesulfinamide

There total 2 articles about N-(1-[(4-methylphenyl)sulfonyl]tetrahydro-1H-pyrrol-2-yl)-2-methyl-2-propanesulfinamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 145472-39-5
1-[(4-methylphenyl)sulfonyl]-2-pyrrolidinol

: 196929-78-9
(R)-2-methylpropane-2-sulfinamide

: 918954-35-5
N-(1-[(4-methylphenyl)sulfonyl]tetrahydro-1H-pyrrol-2-yl)-2-methyl-2-propanesulfinamide

Guidance literature:: With titanium(IV) tetraethanolate; In ethanol; dichloromethane; for 7h; Heating;
DOI:10.1002/anie.200602782

Reference yield:

: 10019-95-1
N-tosylpyrrolidinone

: 918954-35-5
N-(1-[(4-methylphenyl)sulfonyl]tetrahydro-1H-pyrrol-2-yl)-2-methyl-2-propanesulfinamide

Guidance literature:: Multi-step reaction with 2 steps

1: 98 percent / DIBAL-H / CH₂Cl₂ / 1.17 h / -78 - 20 °C

2: 95 percent / Ti(OEt)4 / CH₂Cl₂; ethanol / 7 h / Heating

With titanium(IV) tetraethanolate; diisobutylaluminium hydride; In ethanol; dichloromethane;
DOI:10.1002/anie.200602782