(+/-)-N-[(Z)-2-bromo-3-phenylprop-2-enyl]-N-[1-cyclohexyl-3-(trimethylsilyl)prop-2-ynyl]-4-methylbenzenesulfonamide

Base Information

Chemical Name:(+/-)-N-[(Z)-2-bromo-3-phenylprop-2-enyl]-N-[1-cyclohexyl-3-(trimethylsilyl)prop-2-ynyl]-4-methylbenzenesulfonamide
CAS No.:1342341-16-5
Molecular Formula:C₂₈H₃₆BrNO₂SSi
Molecular Weight:558.655
Hs Code.:

Synonyms:(+/-)-N-[(Z)-2-bromo-3-phenylprop-2-enyl]-N-[1-cyclohexyl-3-(trimethylsilyl)prop-2-ynyl]-4-methylbenzenesulfonamide

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Chemical Property of (+/-)-N-[(Z)-2-bromo-3-phenylprop-2-enyl]-N-[1-cyclohexyl-3-(trimethylsilyl)prop-2-ynyl]-4-methylbenzenesulfonamide

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Technology Process of (+/-)-N-[(Z)-2-bromo-3-phenylprop-2-enyl]-N-[1-cyclohexyl-3-(trimethylsilyl)prop-2-ynyl]-4-methylbenzenesulfonamide

There total 6 articles about (+/-)-N-[(Z)-2-bromo-3-phenylprop-2-enyl]-N-[1-cyclohexyl-3-(trimethylsilyl)prop-2-ynyl]-4-methylbenzenesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 947315-12-0
(+/-)-N-[1-cyclohexyl-3-(trimethylsilyl)prop-2-ynyl]-4-methylbenzenesulfonamide

: 2048-31-9,66820-54-0
(Z)-2-bromo-3-phenylprop-2-en-1-ol

: 1342341-16-5
(+/-)-N-[(Z)-2-bromo-3-phenylprop-2-enyl]-N-[1-cyclohexyl-3-(trimethylsilyl)prop-2-ynyl]-4-methylbenzenesulfonamide

Guidance literature:: With di-isopropyl azodicarboxylate; triphenylphosphine; In tetrahydrofuran; at 0 - 20 ℃;
DOI:10.1055/s-0030-1260098

Reference yield:

: 1342341-15-4
C₂₄H₃₇NO₄SSi

: 1342341-16-5
(+/-)-N-[(Z)-2-bromo-3-phenylprop-2-enyl]-N-[1-cyclohexyl-3-(trimethylsilyl)prop-2-ynyl]-4-methylbenzenesulfonamide

Guidance literature:: Multi-step reaction with 2 steps

1: hydrogenchloride; water / ethyl acetate / 5 h / 50 °C

2: di-isopropyl azodicarboxylate; triphenylphosphine / tetrahydrofuran / 0 - 20 °C

With hydrogenchloride; di-isopropyl azodicarboxylate; water; triphenylphosphine; In tetrahydrofuran; ethyl acetate;
DOI:10.1055/s-0030-1260098

Reference yield:

: 21788-36-3
(Z)-methyl 2-bromo-3-phenylacrylate

: 1342341-16-5
(+/-)-N-[(Z)-2-bromo-3-phenylprop-2-enyl]-N-[1-cyclohexyl-3-(trimethylsilyl)prop-2-ynyl]-4-methylbenzenesulfonamide

Guidance literature:: Multi-step reaction with 2 steps

1: diisobutylaluminium hydride / tetrahydrofuran

2: di-isopropyl azodicarboxylate; triphenylphosphine / tetrahydrofuran / 0 - 20 °C

With di-isopropyl azodicarboxylate; diisobutylaluminium hydride; triphenylphosphine; In tetrahydrofuran;
DOI:10.1055/s-0030-1260098