(+/-)-N-[1-cyclohexyl-3-(trimethylsilyl)prop-2-ynyl]-4-methylbenzenesulfonamide

Base Information

Chemical Name:(+/-)-N-[1-cyclohexyl-3-(trimethylsilyl)prop-2-ynyl]-4-methylbenzenesulfonamide
CAS No.:947315-12-0
Molecular Formula:C₁₉H₂₉NO₂SSi
Molecular Weight:363.596
Hs Code.:

Synonyms:(+/-)-N-[1-cyclohexyl-3-(trimethylsilyl)prop-2-ynyl]-4-methylbenzenesulfonamide

Suppliers and Price of (+/-)-N-[1-cyclohexyl-3-(trimethylsilyl)prop-2-ynyl]-4-methylbenzenesulfonamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (+/-)-N-[1-cyclohexyl-3-(trimethylsilyl)prop-2-ynyl]-4-methylbenzenesulfonamide

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Technology Process of (+/-)-N-[1-cyclohexyl-3-(trimethylsilyl)prop-2-ynyl]-4-methylbenzenesulfonamide

There total 4 articles about (+/-)-N-[1-cyclohexyl-3-(trimethylsilyl)prop-2-ynyl]-4-methylbenzenesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 1342341-15-4
C₂₄H₃₇NO₄SSi

: 947315-12-0
(+/-)-N-[1-cyclohexyl-3-(trimethylsilyl)prop-2-ynyl]-4-methylbenzenesulfonamide

Guidance literature:: With hydrogenchloride; water; In ethyl acetate; at 50 ℃; for 5h;
DOI:10.1055/s-0030-1260098

Reference yield: 74.0%

: 260975-29-9
(E)-N-cyclohexylmethylene-4-toluenesulfonamide

: 1066-54-2
trimethylsilylacetylene

: 947315-12-0
(+/-)-N-[1-cyclohexyl-3-(trimethylsilyl)prop-2-ynyl]-4-methylbenzenesulfonamide

Guidance literature:: With dimethyl zinc(II); In toluene; at 70 ℃; for 24h;
DOI:10.1021/jo070745o

Reference yield:

: 133216-88-3,112497-25-3
(+/-)-1-cyclohexyl-3-(trimethylsilyl)-2-propynol

: 947315-12-0
(+/-)-N-[1-cyclohexyl-3-(trimethylsilyl)prop-2-ynyl]-4-methylbenzenesulfonamide

Guidance literature:: Multi-step reaction with 2 steps

1: di-isopropyl azodicarboxylate; triphenylphosphine / tetrahydrofuran / 20 °C / Cooling

2: hydrogenchloride; water / ethyl acetate / 5 h / 50 °C

With hydrogenchloride; di-isopropyl azodicarboxylate; water; triphenylphosphine; In tetrahydrofuran; ethyl acetate; 1: Mitsunobu reaction;
DOI:10.1055/s-0030-1260098