MoBr₃(C₆H₅P(CH₂CH₂P(C₆H₅)2)2)

Base Information

Chemical Name:MoBr₃(C₆H₅P(CH₂CH₂P(C₆H₅)2)2)
CAS No.:74707-27-0
Molecular Formula:C₃₄H₃₃Br₃MoP₃
Molecular Weight:870.209
Hs Code.:

MoBr<sub>3</sub>(C<sub>6</sub>H<sub>5</sub>P(CH<sub>2</sub>CH<sub>2</sub>P(C<sub>6</sub>H<sub>5</sub>)2)2)

Synonyms:MoBr₃(C₆H₅P(CH₂CH₂P(C₆H₅)2)2)

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Chemical Property of MoBr₃(C₆H₅P(CH₂CH₂P(C₆H₅)2)2)

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Technology Process of MoBr₃(C₆H₅P(CH₂CH₂P(C₆H₅)2)2)

There total 7 articles about MoBr₃(C₆H₅P(CH₂CH₂P(C₆H₅)2)2) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: Mo(N₂)2(C₆H₅P(C₂H₄P(C₆H₅)2)2)P(C₆H₅)3*0.5C₄H₈O

: 74707-27-0
MoBr₃(C₆H₅P(CH₂CH₂P(C₆H₅)2)2)

Guidance literature:: With hydrogen bromide; In tetrahydrofuran; byproducts: NH4Br, N2, P(C6H5)3; THF and HBr condensed into Mo-complex cooled to -196°C; warmed to room temp. and stirred for 24-36 h; pptd.; evapd.; washed with ethanol; dried; elem. anal.;
DOI:10.1021/ja00539a035

Reference yield: 8.0%

: 74707-26-9,75420-24-5
trans-[Mo(N₂)(PhP(CH₂CH₂PPh₂)2)(PPh₃)]

: 74707-27-0
MoBr₃(C₆H₅P(CH₂CH₂P(C₆H₅)2)2)

: 7727-37-9
nitrogen

: 7664-41-7
ammonia

Guidance literature:: With hydrogen bromide; In methanol; complex was treated with anhydrous HCl in THF;
DOI:10.1016/S0020-1693(00)90337-2

Reference yield:

: 74707-26-9,75420-24-5
trans-[Mo(N₂)(PhP(CH₂CH₂PPh₂)2)(PPh₃)]

: 74707-27-0
MoBr₃(C₆H₅P(C₂H₄P(C₆H₅)2)2)

: 302-01-2,78206-91-4,119775-10-9,75013-58-0
hydrazine

Guidance literature:: With hydrogen bromide; In tetrahydrofuran; byproducts: NH4Br, PPh3, N2; liquid HBr added to Mo complex in absence of solvent, added THF, stirred; Kinetics;
DOI:10.1021/ja00358a036