2-(methylthio)methyl-2-benzylmalonic acid

Base Information

Chemical Name:2-(methylthio)methyl-2-benzylmalonic acid
CAS No.:118545-46-3
Molecular Formula:C₁₂H₁₄O₄S
Molecular Weight:254.307
Hs Code.:

Synonyms:2-(methylthio)methyl-2-benzylmalonic acid

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Chemical Property of 2-(methylthio)methyl-2-benzylmalonic acid

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Technology Process of 2-(methylthio)methyl-2-benzylmalonic acid

There total 3 articles about 2-(methylthio)methyl-2-benzylmalonic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 860366-96-7
diethyl 2-benzyl-2-(methylthiomethyl)malonate

: 118545-46-3
2-(methylthio)methyl-2-benzylmalonic acid

Guidance literature:: diethyl 2-benzyl-2-(methylthiomethyl)malonate; With potassium hydroxide; In methanol; water; at 100 ℃; for 4h;

With hydrogenchloride; In methanol; water; pH=1;

Reference yield:

: 607-81-8
diethyl 2-benzylmalonate

: 118545-46-3
2-(methylthio)methyl-2-benzylmalonic acid

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 18 h / 0 - 23 °C

2.1: potassium hydroxide / water; methanol / 4 h / 100 °C

2.2: pH 1

With sodium hydride; potassium hydroxide; In methanol; water; N,N-dimethyl-formamide; mineral oil;

Reference yield:

: 2373-51-5
chloro-methylsulfanyl-methane

: 607-81-8
diethyl 2-benzylmalonate

: 118545-46-3
2-(methylthio)methyl-2-benzylmalonic acid

Guidance literature:: With potassium hydroxide; sodium ethanolate; Yield given. Multistep reaction; 1.) ethanol, 80 deg C, 30 min, 2.) methanol, reflux, 4 h;