2,2,4,4-tetramethyl-3-(phenylimino)-1-methylenecyclobutane

Base Information

Chemical Name:2,2,4,4-tetramethyl-3-(phenylimino)-1-methylenecyclobutane
CAS No.:36332-23-7
Molecular Formula:C₁₅H₁₉N
Molecular Weight:213.323
Hs Code.:

Synonyms:2,2,4,4-tetramethyl-3-(phenylimino)-1-methylenecyclobutane

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Chemical Property of 2,2,4,4-tetramethyl-3-(phenylimino)-1-methylenecyclobutane

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Technology Process of 2,2,4,4-tetramethyl-3-(phenylimino)-1-methylenecyclobutane

There total 6 articles about 2,2,4,4-tetramethyl-3-(phenylimino)-1-methylenecyclobutane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 20019-11-8
2,2,4,4-tetramethyl-3-methylenecyclobutan-1-one

: 62-53-3
aniline

: 36332-23-7
2,2,4,4-tetramethyl-3-(phenylimino)-1-methylenecyclobutane

Guidance literature:: With toluene-4-sulfonic acid; In toluene; Heating;
DOI:10.1021/ol0102693

Reference yield:

: 933-52-8
2,2,4,4-tetramethyl-1,3-cyclobutanedione

: 36332-23-7
2,2,4,4-tetramethyl-3-(phenylimino)-1-methylenecyclobutane

Guidance literature:: Multi-step reaction with 2 steps

1: 60 percent / p-TsOH*H₂O / benzene / 6 h / Heating

2: 1.) t-BuOK / 1.) t-BuOH, ether, RT, 1 h, 2.) t-BuOH, ether, overnight

With potassium tert-butylate; toluene-4-sulfonic acid; In benzene;
DOI:10.1021/ja00152a010