2-Benzyloxycarbonylamino-4-(dimethoxy-phosphoryl)-butyric acid methyl ester

Base Information

• Chemical Name: 2-Benzyloxycarbonylamino-4-(dimethoxy-phosphoryl)-butyric acid methyl ester
• CAS No.: 208997-79-9
• Molecular Formula: C₁₅H₂₂NO₇P
• Molecular Weight: 359.316

Synonyms:2-Benzyloxycarbonylamino-4-(dimethoxy-phosphoryl)-butyric acid methyl ester

Chemical Property of 2-Benzyloxycarbonylamino-4-(dimethoxy-phosphoryl)-butyric acid methyl ester

Chemical Property:

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Technology Process of 2-Benzyloxycarbonylamino-4-(dimethoxy-phosphoryl)-butyric acid methyl ester

There total 1 articles about 2-Benzyloxycarbonylamino-4-(dimethoxy-phosphoryl)-butyric acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

diazomethane (186581-53-3,908094-01-9,334-88-3) + 2-(N-benzyloxycarbonylamino)-4-phosphonobutanoic acid (155179-92-3) → 2-Benzyloxycarbonylamino-4-(dimethoxy-phosphoryl)-butyric acid methyl ester (208997-79-9)

Guidance literature:

With methanol; In diethyl ether;

DOI:10.1006/bioo.1997.1077

Reference yield: 90.0%

2-Benzyloxycarbonylamino-4-(dimethoxy-phosphoryl)-butyric acid methyl ester (208997-79-9) → methyl hydrogen (RS) 3-(benzyloxycarbonylamino)-3-(methoxycarbonyl)-propylphosphonate (208997-82-4)

Guidance literature:

With tert-butylamine; for 96h; Heating;

DOI:10.1006/bioo.1997.1077

Reference yield: 80.0%

2-Benzyloxycarbonylamino-4-(dimethoxy-phosphoryl)-butyric acid methyl ester (208997-79-9) → 2-Benzyloxycarbonylamino-4-(dimethoxy-phosphoryl)-butyric acid

Guidance literature:

With sodium hydroxide; In ethanol; for 1h; Ambient temperature;

DOI:10.1006/bioo.1997.1077

upstream raw materials:

diazomethane

2-(N-benzyloxycarbonylamino)-4-phosphonobutanoic acid

Downstream raw materials:

methyl hydrogen (RS) 3-(benzyloxycarbonylamino)-3-(methoxycarbonyl)-propylphosphonate

DL-methyl {3-[(benzyloxycarbonyl)amino]-3-methoxycarbonylpropyl}-SR-phosphonamidate

DL-methyl N-ethyl-{3-[(benzyloxycarbonyl)amino]-3-methoxycarbonylpropyl}-SR-phosphonamidate

DL-methyl N,N-dimethyl-{3-[(benzyloxycarbonyl)amino]-3-methoxycarbonylpropyl}-SR-phosphonamidate

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