methyl hydrogen (RS) 3-(benzyloxycarbonylamino)-3-(methoxycarbonyl)-propylphosphonate

Base Information

Chemical Name:methyl hydrogen (RS) 3-(benzyloxycarbonylamino)-3-(methoxycarbonyl)-propylphosphonate
CAS No.:208997-82-4
Molecular Formula:C₁₄H₂₀NO₇P
Molecular Weight:345.289
Hs Code.:

Synonyms:methyl hydrogen (RS) 3-(benzyloxycarbonylamino)-3-(methoxycarbonyl)-propylphosphonate

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Chemical Property of methyl hydrogen (RS) 3-(benzyloxycarbonylamino)-3-(methoxycarbonyl)-propylphosphonate

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Technology Process of methyl hydrogen (RS) 3-(benzyloxycarbonylamino)-3-(methoxycarbonyl)-propylphosphonate

There total 1 articles about methyl hydrogen (RS) 3-(benzyloxycarbonylamino)-3-(methoxycarbonyl)-propylphosphonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 208997-79-9
2-Benzyloxycarbonylamino-4-(dimethoxy-phosphoryl)-butyric acid methyl ester

: 208997-82-4
methyl hydrogen (RS) 3-(benzyloxycarbonylamino)-3-(methoxycarbonyl)-propylphosphonate

Guidance literature:: With tert-butylamine; for 96h; Heating;
DOI:10.1006/bioo.1997.1077

Reference yield:

: 208997-82-4
methyl hydrogen (RS) 3-(benzyloxycarbonylamino)-3-(methoxycarbonyl)-propylphosphonate

: C₁₄H₁₉ClNO₆P

Guidance literature:: With oxalyl dichloride; N,N-dimethyl-formamide; In dichloromethane; a) 0 deg C, 20 min, b) RT, 1.5 h;
DOI:10.1006/bioo.1997.1077

Reference yield:

: 208997-82-4
methyl hydrogen (RS) 3-(benzyloxycarbonylamino)-3-(methoxycarbonyl)-propylphosphonate

: 208997-91-5
DL-methyl N,N-dimethyl-{3-[(benzyloxycarbonyl)amino]-3-methoxycarbonylpropyl}-SR-phosphonamidate

Guidance literature:: Multi-step reaction with 2 steps

1: oxalyl chloride, DMF / CH₂Cl₂ / a) 0 deg C, 20 min, b) RT, 1.5 h

2: tetrahydrofuran; CH₂Cl₂ / Ambient temperature

With oxalyl dichloride; N,N-dimethyl-formamide; In tetrahydrofuran; dichloromethane;
DOI:10.1006/bioo.1997.1077