2,6-dideoxy-2,6-(trifluoroacetimido)-D-glycero-D-ido-heptononitrile 3,4,5,7-tetrabenzoate

Base Information

Chemical Name:2,6-dideoxy-2,6-(trifluoroacetimido)-D-glycero-D-ido-heptononitrile 3,4,5,7-tetrabenzoate
CAS No.:120172-78-3
Molecular Formula:C₃₇H₂₇F₃N₂O₉
Molecular Weight:700.625
Hs Code.:

Synonyms:2,6-dideoxy-2,6-(trifluoroacetimido)-D-glycero-D-ido-heptononitrile 3,4,5,7-tetrabenzoate

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Chemical Property of 2,6-dideoxy-2,6-(trifluoroacetimido)-D-glycero-D-ido-heptononitrile 3,4,5,7-tetrabenzoate

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Technology Process of 2,6-dideoxy-2,6-(trifluoroacetimido)-D-glycero-D-ido-heptononitrile 3,4,5,7-tetrabenzoate

There total 4 articles about 2,6-dideoxy-2,6-(trifluoroacetimido)-D-glycero-D-ido-heptononitrile 3,4,5,7-tetrabenzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.1%

: 120172-77-2
2,6-dideoxy-2,6-imino-D-glycero-D-ido-heptononitrile 3,4,5,7-tetrabenzoate

: 120172-78-3
2,6-dideoxy-2,6-(trifluoroacetimido)-D-glycero-D-ido-heptononitrile 3,4,5,7-tetrabenzoate

Guidance literature:: With triethylamine; trifluoroacetic anhydride; In methanol; ice-water; ethyl acetate;

Reference yield: 89.0%

: 120172-77-2
2,6-dideoxy-2,6-imino-D-glycero-D-ido-heptononitrile 3,4,5,7-tetrabenzoate

: 407-25-0
trifluoroacetic anhydride

: 120172-78-3
2,6-dideoxy-2,6-(trifluoroacetimido)-D-glycero-D-ido-heptononitrile 3,4,5,7-tetrabenzoate

Guidance literature:: With triethylamine; In ethyl acetate; 1.) 0 deg C, 1 h, 2.) room temperature, 21 h;
DOI:10.1021/jo00272a015

Reference yield:

: 78821-34-8
2,6-dideoxy-2,6-imino-D-glycero-D-ido-heptononitrile

: 120172-78-3
2,6-dideoxy-2,6-(trifluoroacetimido)-D-glycero-D-ido-heptononitrile 3,4,5,7-tetrabenzoate

Guidance literature:: Multi-step reaction with 2 steps

1: 82 percent / triethylamine / ethyl acetate / 18 h / Ambient temperature

2: 89 percent / triethylamine / ethyl acetate / 1.) 0 deg C, 1 h, 2.) room temperature, 21 h

With triethylamine; In ethyl acetate;
DOI:10.1021/jo00272a015